2,4-Dihydroxy-6-methoxyphenyl-3,4-dimethoxybenzyl ketone

Base Information

• Chemical Name: 2,4-Dihydroxy-6-methoxyphenyl-3,4-dimethoxybenzyl ketone
• CAS No.: 109092-83-3
• Molecular Formula: C₁₇H₁₈O₆
• Molecular Weight: 318.326
• Mol file: 109092-83-3.mol

Synonyms:

Chemical Property of 2,4-Dihydroxy-6-methoxyphenyl-3,4-dimethoxybenzyl ketone

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 2,4-Dihydroxy-6-methoxyphenyl-3,4-dimethoxybenzyl ketone

There total 1 articles about 2,4-Dihydroxy-6-methoxyphenyl-3,4-dimethoxybenzyl ketone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

5-methoxyresorcinol (2174-64-3) + 3,4-dimethoxyphenylacetonitrile (93-17-4) → 2,4-Dihydroxy-6-methoxyphenyl-3,4-dimethoxybenzyl ketone (109092-83-3)

Guidance literature:

With hydrogenchloride; diethyl ether; zinc(II) chloride; und Erhitzen des Reaktionsprodukts mit Wasser;

DOI:10.1039/jr9490001571

Reference yield:

2,4-Dihydroxy-6-methoxyphenyl-3,4-dimethoxybenzyl ketone (109092-83-3) → 2,4,5-Trihydroxy-6-methoxyphenyl-3,4-dimethoxybenzyl ketone (129207-80-3)

Guidance literature:

With potassium peroxomonosulphate; In potassium hydroxide; Ambient temperature;

Reference yield:

2,4-Dihydroxy-6-methoxyphenyl-3,4-dimethoxybenzyl ketone (109092-83-3) → 2-Hydroxy-4,5-methylenedioxy-6-methoxyphenyl-3,4-dimethoxybenzyl ketone (2631-85-8)

Guidance literature:

Multi-step reaction with 2 steps

1: aq. potassium persulphate / aq. KOH / Ambient temperature

2: K₂CO₃ / acetone / 45 h / Heating

With potassium peroxomonosulphate; potassium carbonate; In potassium hydroxide; acetone;

upstream raw materials:

5-methoxyresorcinol

3,4-dimethoxyphenylacetonitrile

Downstream raw materials:

3-(3,4-dimethoxy-phenyl)-4,7-dihydroxy-5-methoxy-coumarin

2-(3,4-dimethoxyphenyl)-1-(2-hydroxy-4,6-dimethoxyphenyl)ethanone

2,4,5-Trihydroxy-6-methoxyphenyl-3,4-dimethoxybenzyl ketone

2-Hydroxy-4,5-methylenedioxy-6-methoxyphenyl-3,4-dimethoxybenzyl ketone