TiCl₄(4-t-BuC₆H₄CH₂PPh₂=NC₆H₂Me₃-2,4,6)

Base Information

Chemical Name:TiCl₄(4-t-BuC₆H₄CH₂PPh₂=NC₆H₂Me₃-2,4,6)
CAS No.:388123-79-3
Molecular Formula:C₃₂H₃₆Cl₄NPTi
Molecular Weight:655.31
Hs Code.:

TiCl<sub>4</sub>(4-t-BuC<sub>6</sub>H<sub>4</sub>CH<sub>2</sub>PPh<sub>2</sub>=NC<sub>6</sub>H<sub>2</sub>Me<sub>3</sub>-2,4,6)

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Suppliers and Price of TiCl₄(4-t-BuC₆H₄CH₂PPh₂=NC₆H₂Me₃-2,4,6)

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of TiCl₄(4-t-BuC₆H₄CH₂PPh₂=NC₆H₂Me₃-2,4,6)

Chemical Property:

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Technology Process of TiCl₄(4-t-BuC₆H₄CH₂PPh₂=NC₆H₂Me₃-2,4,6)

There total 1 articles about TiCl₄(4-t-BuC₆H₄CH₂PPh₂=NC₆H₂Me₃-2,4,6) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 63.0%

: 7550-45-0
titanium tetrachloride

: 388123-78-2
4-t-BuC₆H₄CH₂PPh₂=NC₆H₂Me₃-2,4,6

: 388123-79-3
TiCl₄(4-t-BuC₆H₄CH₂PPh₂=NC₆H₂Me₃-2,4,6)

Guidance literature:: In toluene; under N2, Schlenk techniques; 1 equiv. of TiCl4 in toluene added dropwise over 15 min to soln. of ligand in toluene at -78°C; 30 min; ppt. collected at low temp.; dried under vac.; warmed to ambient temp.; elem. anal.;
DOI:10.1039/b105038a

Reference yield:

: 388123-79-3
TiCl₄(4-t-BuC₆H₄CH₂PPh₂=NC₆H₂Me₃-2,4,6)

: 388123-80-6
TiCl₃(4-t-BuC₆H₄CHPPh₂=NC₆H₂Me₃-2,4,6)

Guidance literature:: In ⁽²⁾H₈-toluene; byproducts: HCl; under N2, Schlenk techniques; soln. of Ti complex in toluene-d8 heated to 30°C; not isolated; detd. by (31)P NMR spectroscopy;
DOI:10.1039/b105038a

Reference yield:

: 388123-79-3
TiCl₄(4-t-BuC₆H₄CH₂PPh₂=NC₆H₂Me₃-2,4,6)

: 121-44-8
triethylamine

: 39478-32-5
TiCl₄(N(C₂H₅)3)2

: 388123-80-6
TiCl₃(4-t-BuC₆H₄CHPPh₂=NC₆H₂Me₃-2,4,6)

Guidance literature:: In ⁽²⁾H₈-toluene; under N2, Schlenk techniques; Et3N added to soln. of Ti complex in toluene-d8 (up to 0°C); warmed to room temp.; not isolated; detd. by (31)P NMR spectroscopy;
DOI:10.1039/b105038a