Technology Process of C33H24F10O6
There total 3 articles about C33H24F10O6 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
Multi-step reaction with 2 steps
1.1: 85 percent / Et3N / dimethylformamide / 1 h
2.1: PPh3; DIAD / tetrahydrofuran / Heating
2.2: PPh3; DIAD / tetrahydrofuran / Heating
With
di-isopropyl azodicarboxylate; triethylamine; triphenylphosphine;
In
tetrahydrofuran; N,N-dimethyl-formamide;
2.1: Mitsunobu reaction / 2.2: Mitsunobu reaction;
DOI:10.1021/jo070568r
- Guidance literature:
-
Multi-step reaction with 2 steps
1.1: 85 percent / Et3N / dimethylformamide / 1 h
2.1: PPh3; DIAD / tetrahydrofuran / Heating
2.2: PPh3; DIAD / tetrahydrofuran / Heating
With
di-isopropyl azodicarboxylate; triethylamine; triphenylphosphine;
In
tetrahydrofuran; N,N-dimethyl-formamide;
2.1: Mitsunobu reaction / 2.2: Mitsunobu reaction;
DOI:10.1021/jo070568r
- Guidance literature:
-
C22H8F10O6; 5-hexyl-1-ol;
With
di-isopropyl azodicarboxylate; triphenylphosphine;
In
tetrahydrofuran;
Heating;
n-Pent-4-enyl alcohol;
With
di-isopropyl azodicarboxylate; triphenylphosphine;
In
tetrahydrofuran;
Further stages.;
Heating;
DOI:10.1021/jo070568r