nickel(II) bis(2-mercapto-3-trimethylsilylphenyl)sulfide diphenylsulfimine

Base Information

Chemical Name:nickel(II) bis(2-mercapto-3-trimethylsilylphenyl)sulfide diphenylsulfimine
CAS No.:828919-16-0
Molecular Formula:C₃₀H₃₅NNiS₄Si₂
Molecular Weight:652.74
Hs Code.:

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Chemical Property of nickel(II) bis(2-mercapto-3-trimethylsilylphenyl)sulfide diphenylsulfimine

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Technology Process of nickel(II) bis(2-mercapto-3-trimethylsilylphenyl)sulfide diphenylsulfimine

There total 1 articles about nickel(II) bis(2-mercapto-3-trimethylsilylphenyl)sulfide diphenylsulfimine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 78.0%

: S,S'-diphenylsulfimide monohydrate

: 472958-11-5
tri[nickel(II) bis(2-mercapto-3-trimethylsilylphenyl)sulfide]

: 828919-16-0
nickel(II) bis(2-mercapto-3-trimethylsilylphenyl)sulfide diphenylsulfimine

Guidance literature:: In tetrahydrofuran; (N2, at room temp.), ligand added to Ni complex in THF, stirred for 12 h; concd., layered with pentane, pptd. at -25°C for 7 d, washed (pentane), dried (vac.), elem. anal.;
DOI:10.1002/ejic.200300786

Reference yield:

: 828919-16-0
nickel(II) bis(2-mercapto-3-trimethylsilylphenyl)sulfide diphenylsulfimine

: 16873-17-9,12184-84-8
deuterium

: nickel(II) bis(2-mercapto-3-trimethylsilylphenyl)sulfide diphenylsulfimine

Guidance literature:: In tetrahydrofuran-d8; water; byproducts: HD; High Pressure; (in a high pressure NMR tube), concd. soln. of Ni complex in THF-d8 treated with H2O, pressurized with 18 bar of D2 for 80-120 h; not isolated, detected by NMR;
DOI:10.1002/ejic.200300786

Reference yield:

: 828919-16-0
nickel(II) bis(2-mercapto-3-trimethylsilylphenyl)sulfide diphenylsulfimine

: 201230-82-2
carbon monoxide

: nickel(II) bis(2-mercapto-3-trimethylsilylphenyl)sulfide CO diphenylsulfimine

Guidance literature:: In dichloromethane; CO bubbled through soln. of Ni complex at 20°C (1 bar of CO); not isolated, detected by IR, NMR;
DOI:10.1002/ejic.200300786