deoxycytidylyl-(3',5')-guanosine sodium salt

Base Information

Chemical Name:deoxycytidylyl-(3',5')-guanosine sodium salt
CAS No.:110497-28-4
Molecular Formula:C₁₉H₂₄N₈O₁₀P*Na
Molecular Weight:578.411
Hs Code.:

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Chemical Property of deoxycytidylyl-(3',5')-guanosine sodium salt

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Technology Process of deoxycytidylyl-(3',5')-guanosine sodium salt

There total 7 articles about deoxycytidylyl-(3',5')-guanosine sodium salt which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1053743-24-0
4-oxo-pentanoic acid 2-{[2-acetoxymethyl-5-(4-benzoylamino-2-oxo-2H-pyrimidin-1-yl)-tetrahydro-furan-3-yloxy]-cyanomethylsulfanyl-phosphoryloxymethyl}-5-[6-(2,5-dichloro-phenoxy)-2-isobutyrylamino-purin-9-yl]-tetrahydro-furan-3-yl ester

: 110497-28-4
deoxycytidylyl-(3',5')-guanosine sodium salt

Guidance literature:: 4-oxo-pentanoic acid 2-{[2-acetoxymethyl-5-(4-benzoylamino-2-oxo-2H-pyrimidin-1-yl)-tetrahydro-furan-3-yloxy]-cyanomethylsulfanyl-phosphoryloxymethyl}-5-[6-(2,5-dichloro-phenoxy)-2-isobutyrylamino-purin-9-yl]-tetrahydro-furan-3-yl ester; With (E)-2-nitrobenzaldehyde oxime; N,N,N',N'-tetramethylguanidine; In dichloromethane; acetonitrile; at 20 ℃; for 16h;

With ammonium hydroxide; at 55 ℃; for 15h;

With Amberlite IR 120 (Na+ form); In water;
DOI:10.1016/S0040-4039(03)00322-8

Reference yield:

: C₃₇H₃₅N₃O₉P^(1-)

: 110497-28-4
deoxycytidylyl-(3',5')-guanosine sodium salt

Guidance literature:: Multi-step reaction with 6 steps

1.1: (PhO)2POCl; C₅H₅N / 20 °C

2.1: Cl₂CHCO₂H; pyrrole / CH₂Cl₂ / 20 °C

3.1: C₅H₅N / 20 °C

4.1: DBU / CH₂Cl₂ / 0.5 h / 20 °C

5.1: CF₃CO₂H / CH₂Cl₂ / 0.08 h / 20 °C

5.2: PhNMe₂ / CH₂Cl₂ / 15 h / 20 °C

6.1: E-2-nitrobenzaldoxime; (Me₂N)2C=NH / acetonitrile; CH₂Cl₂ / 16 h / 20 °C

6.2: aq. NH₃ / 15 h / 55 °C

6.3: Amberlite IR 120 (Na+ form) / H₂O

With pyridine; dichloro-acetic acid; pyrrole; (E)-2-nitrobenzaldehyde oxime; 1,8-diazabicyclo[5.4.0]undec-7-ene; chlorophosphoric acid diphenyl ester; trifluoroacetic acid; N,N,N',N'-tetramethylguanidine; In dichloromethane; acetonitrile;
DOI:10.1016/S0040-4039(03)00322-8

Reference yield:

: 199436-66-3
2'-deoxy-6-O-(2,5-dichlorophenyl)-2-N-isobutyryl-3'-O-levulinylguanosine

: 110497-28-4
deoxycytidylyl-(3',5')-guanosine sodium salt

Guidance literature:: Multi-step reaction with 6 steps

1.1: (PhO)2POCl; C₅H₅N / 20 °C

2.1: Cl₂CHCO₂H; pyrrole / CH₂Cl₂ / 20 °C

3.1: C₅H₅N / 20 °C

4.1: DBU / CH₂Cl₂ / 0.5 h / 20 °C

5.1: CF₃CO₂H / CH₂Cl₂ / 0.08 h / 20 °C

5.2: PhNMe₂ / CH₂Cl₂ / 15 h / 20 °C

6.1: E-2-nitrobenzaldoxime; (Me₂N)2C=NH / acetonitrile; CH₂Cl₂ / 16 h / 20 °C

6.2: aq. NH₃ / 15 h / 55 °C

6.3: Amberlite IR 120 (Na+ form) / H₂O

With pyridine; dichloro-acetic acid; pyrrole; (E)-2-nitrobenzaldehyde oxime; 1,8-diazabicyclo[5.4.0]undec-7-ene; chlorophosphoric acid diphenyl ester; trifluoroacetic acid; N,N,N',N'-tetramethylguanidine; In dichloromethane; acetonitrile;
DOI:10.1016/S0040-4039(03)00322-8