trans-[MnBr(CO)2(dppe)(P(OPh)3)]

Base Information

Chemical Name:trans-[MnBr(CO)2(dppe)(P(OPh)3)]
CAS No.:38100-16-2
Molecular Formula:C₄₆H₃₉BrMnO₅P₃
Molecular Weight:899.576
Hs Code.:

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of trans-[MnBr(CO)2(dppe)(P(OPh)3)]

Chemical Property:

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Technology Process of trans-[MnBr(CO)2(dppe)(P(OPh)3)]

There total 2 articles about trans-[MnBr(CO)2(dppe)(P(OPh)3)] which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 38100-16-2,79814-03-2
cis,cis-[MnBr(CO)2(dppe)(P(OPh)3)]

: 38100-16-2,79814-03-2
trans-[MnBr(CO)2(dppe)(P(OPh)3)]

Guidance literature:: With NO₂; In dichloromethane; NO2 was bubbled through the soln. of the educt under N2; excess NO2 was removed by bubbling through N2 and addn. of 80 % hydrazine*H2O, filtration, evapn. to dryness, the product was wsahed with hexane and recrystd. from CH2Cl2/hexane; elem. anal.;
DOI:10.1039/DT9810002049

Reference yield:

: 101-02-0
triphenyl phosphite

: 37523-64-1
fac-[bromo(1,2-bis(diphenylphosphino)ethane)tricarbonylmanganese(I)]

: 38100-16-2,79814-03-2
cis,cis-[MnBr(CO)2(dppe)(P(OPh)3)]

Guidance literature:: In toluene; 0.5 h, reflux, under N2; the solvent was removed in vac., pptn. by addn. of hexane, the product was recrystd. from CH2Cl2/ethanol; elem. anal.;
DOI:10.1039/DT9810002049

Reference yield:

: 38100-16-2,79814-03-2
cis,cis-[MnBr(CO)2(dppe)(P(OPh)3)]

: 38100-16-2,79814-03-2
trans-[MnBr(CO)2(dppe)(P(OPh)3)]

Guidance literature:: With NO₂; In dichloromethane; NO2 was bubbled through the soln. of the educt under N2; excess NO2 was removed by bubbling through N2 and addn. of 80 % hydrazine*H2O, filtration, evapn. to dryness, the product was wsahed with hexane and recrystd. from CH2Cl2/hexane; elem. anal.;
DOI:10.1039/DT9810002049