[NEt₄][Ru(CN)(CO)2(PPh₃)(tetrachloro-o-catecholate)]

Base Information

Chemical Name:[NEt₄][Ru(CN)(CO)2(PPh₃)(tetrachloro-o-catecholate)]
CAS No.:943150-63-8
Molecular Formula:C₈H₂₀N*C₂₇H₁₅Cl₄NO₄PRu
Molecular Weight:821.53
Hs Code.:

[NEt<sub>4</sub>][Ru(CN)(CO)2(PPh<sub>3</sub>)(tetrachloro-o-catecholate)]

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of [NEt₄][Ru(CN)(CO)2(PPh₃)(tetrachloro-o-catecholate)]

Chemical Property:

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Technology Process of [NEt₄][Ru(CN)(CO)2(PPh₃)(tetrachloro-o-catecholate)]

There total 1 articles about [NEt₄][Ru(CN)(CO)2(PPh₃)(tetrachloro-o-catecholate)] which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 68.0%

: [(Ru(CO)2(PPh3)(μ-tetrachloro-o-catecholate))2]

: 13435-20-6
tetraethylammoniumcyanide

: 943150-63-8
[NEt₄][Ru(CN)(CO)2(PPh₃)(tetrachloro-o-catecholate)]

Guidance literature:: In dichloromethane; under N2; Et4NCN added to soln. of Ru complex in CH2Cl2, mixt. stirred for 10 min; soln. filtered, hexane added, soln. concd. under vac. to complete pptn.,solid dissolved in CH2Cl2, filtered, n-hexane added to filtrate, concd. under vac.; elem. anal.;
DOI:10.1039/b700648a

Reference yield: 76.0%

: 110-54-3
hexane

: 943150-63-8
[NEt₄][Ru(CN)(CO)2(PPh₃)(tetrachloro-o-catecholate)]

: [(Ru(CO)2(P(OPh)3)(μ-tetrachloro-o-catecholate))2]

: [NEt4][Ru2(μ-CN)(CO)4(PPh3)(P(OPh)3)(tetrachloro-o-catecholate)2]*0.5(hexane)

Guidance literature:: In dichloromethane; under N2; Ru complex salt added to soln. of dinuclear Ru complex in CH2Cl2 under stirring, mixt. stirred for 10 min; soln. filtered, hexane added to filtrate, concd. under vac. to complete pptn., re-pptn. from CH2Cl2/hexane; elem. anal.;
DOI:10.1039/b700648a

Reference yield: 54.0%

: [Mo(CO)2(η-PhCCPh)(hydrotris(3,5-dimethylpyrazolyl)borate)][PF6]

: 943150-63-8
[NEt₄][Ru(CN)(CO)2(PPh₃)(o-O₂C₆Cl₄)]

: 943150-17-2,943150-12-7
[(o-O2C6Cl4)(Ph3P)(OC)2Ru(μ-CN)Mo(CO)(PhCCPh)(hydrotris(3,5-dimethylpyrazolyl)borate)]

Guidance literature:: In dichloromethane; addn. of Ru complex to a stirred soln. of Mo complex in CH2Cl2 under N2,standing for 15 min; removal of solvent, addn. of toluene, filtration through Celite, concn.,addn. of hexane, elem. anal.;
DOI:10.1039/b700549k