Technology Process of C48H59N8O5P
There total 5 articles about C48H59N8O5P which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
(C3N2HCH3COCHC3H7NH2NCHC3H7CO)2;
With
caesium carbonate;
In
acetonitrile;
at 90 ℃;
for 0.166667h;
bis[m-(bromomethyl)phenyl]phenylphosphane oxide;
In
acetonitrile;
for 1h;
Reflux;
DOI:10.1002/chem.201002073
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: magnesium / tetrahydrofuran / 1 h / Reflux
1.2: 1 h / 20 °C
2.1: dihydrogen peroxide / tetrahydrofuran; water / 20 °C
3.1: N-Bromosuccinimide; 2,2'-azobis(isobutyronitrile) / tetrachloromethane / 9 h / Reflux; UV-irradiation
4.1: caesium carbonate / acetonitrile / 0.17 h / 90 °C
4.2: 1 h / Reflux
With
N-Bromosuccinimide; 2,2'-azobis(isobutyronitrile); dihydrogen peroxide; caesium carbonate; magnesium;
In
tetrahydrofuran; tetrachloromethane; water; acetonitrile;
DOI:10.1002/chem.201002073
- Guidance literature:
-
Multi-step reaction with 2 steps
1.1: N-Bromosuccinimide; 2,2'-azobis(isobutyronitrile) / tetrachloromethane / 9 h / Reflux; UV-irradiation
2.1: caesium carbonate / acetonitrile / 0.17 h / 90 °C
2.2: 1 h / Reflux
With
N-Bromosuccinimide; 2,2'-azobis(isobutyronitrile); caesium carbonate;
In
tetrachloromethane; acetonitrile;
DOI:10.1002/chem.201002073