CH₃Ir(OSO₂CF₃)2(CO)((C₆H₅)2PCH₂CH₂P(C₆H₅)2)

Base Information

Chemical Name:CH₃Ir(OSO₂CF₃)2(CO)((C₆H₅)2PCH₂CH₂P(C₆H₅)2)
CAS No.:175230-91-8
Molecular Formula:C₃₀H₂₇F₆IrO₇P₂S₂
Molecular Weight:931.83
Hs Code.:

CH<sub>3</sub>Ir(OSO<sub>2</sub>CF<sub>3</sub>)2(CO)((C<sub>6</sub>H<sub>5</sub>)2PCH<sub>2</sub>CH<sub>2</sub>P(C<sub>6</sub>H<sub>5</sub>)2)

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Suppliers and Price of CH₃Ir(OSO₂CF₃)2(CO)((C₆H₅)2PCH₂CH₂P(C₆H₅)2)

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of CH₃Ir(OSO₂CF₃)2(CO)((C₆H₅)2PCH₂CH₂P(C₆H₅)2)

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Technology Process of CH₃Ir(OSO₂CF₃)2(CO)((C₆H₅)2PCH₂CH₂P(C₆H₅)2)

There total 1 articles about CH₃Ir(OSO₂CF₃)2(CO)((C₆H₅)2PCH₂CH₂P(C₆H₅)2) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 85421-68-7
IrI(CO)(1,2-bis(diphenylphosphino)ethane)

: 175230-91-8
CH₃Ir(OSO₂CF₃)2(CO)((C₆H₅)2PCH₂CH₂P(C₆H₅)2)

Guidance literature:: Multi-step reaction with 2 steps

1: methyl iodide / dichloromethane

2: dichloromethane

With methyl iodide; In dichloromethane;
DOI:10.1016/0020-1693(95)04527-9

Reference yield: 60.0%

: 175230-91-8
CH₃Ir(OSO₂CF₃)2(CO)((C₆H₅)2PCH₂CH₂P(C₆H₅)2)

: 175230-92-9
IrH(CO)(SO₃CF₃)2((C₆H₅)2PC₂H₄P(C₆H₅)2)

Guidance literature:: With H₂; In dichloromethane; byproducts: CH4; H2 addn. to degassed Ir-compd. soln., soln. stirring 5 min, hexane addn. under H2, soln. vol. redn. under H2 flow, pptn.; crystals isolation (glass frit), recrystn. from CH2Cl2/hexane; elem. anal.;
DOI:10.1016/0020-1693(95)04527-9

Reference yield:

: 175230-91-8
CH₃Ir(OSO₂CF₃)2(CO)((C₆H₅)2PCH₂CH₂P(C₆H₅)2)

: 615-42-9
1,2-Diiodobenzene

: 79060-88-1
sodium tetrakis[(3,5-di-trifluoromethyl)phenyl]borate

: [Ir(Me)(CO)(dppe)(DIB)][BArf₄]2

Guidance literature:: In dichloromethane; byproducts: CF3SO3Na; reaction of iridium complex with excess of boron compd. in CH2Cl2; filtration, evapn.;
DOI:10.1021/ja016127l