trans-[(1,2-diphenyl-1,2-dicyclopentadienyl)ethanediyl]iron(II)

Base Information

Chemical Name:trans-[(1,2-diphenyl-1,2-dicyclopentadienyl)ethanediyl]iron(II)
CAS No.:114357-30-1
Molecular Formula:C₂₄H₂₀Fe
Molecular Weight:364.27
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Chemical Property of trans-[(1,2-diphenyl-1,2-dicyclopentadienyl)ethanediyl]iron(II)

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Technology Process of trans-[(1,2-diphenyl-1,2-dicyclopentadienyl)ethanediyl]iron(II)

There total 1 articles about trans-[(1,2-diphenyl-1,2-dicyclopentadienyl)ethanediyl]iron(II) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 52.0%

: 94553-82-9
Fe(η6-C6H6)(PMe3)2

: 7338-50-3
6-phenylfulvene

: 114357-30-1,195723-96-7
trans-[(1,2-diphenyl-1,2-dicyclopentadienyl)ethanediyl]iron(II)

Guidance literature:: In light petroleum; a soln. of Fe-complex in light petroleum was treated with a soln. of anexcess of fulvene in light petroleum at -20°C under N2 atmosphere, mixt. was stirred for 2 h; volatiles were removed in vacuo at 40°C, residue was extd. with light petroleum, filtered, filtrate concd., chromd. on an alumina column(eluent light petroleum), crystd. from light petroleum; elem. anal.;
DOI:10.1039/DT9870002031