1-(3-hydroxy-4-carboxyphenyl)-4-carboxy-5-phenyl-1H-1,2,3-triazole

Base Information

Chemical Name:1-(3-hydroxy-4-carboxyphenyl)-4-carboxy-5-phenyl-1H-1,2,3-triazole
CAS No.:87878-05-5
Molecular Formula:C₁₆H₁₁N₃O₅
Molecular Weight:325.28
Hs Code.:

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1-(3-hydroxy-4-carboxyphenyl)-4-carboxy-5-phenyl-1H-1,2,3-triazole

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Technology Process of 1-(3-hydroxy-4-carboxyphenyl)-4-carboxy-5-phenyl-1H-1,2,3-triazole

There total 4 articles about 1-(3-hydroxy-4-carboxyphenyl)-4-carboxy-5-phenyl-1H-1,2,3-triazole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 66761-27-1
4-carboxy-3-hydroxyphenyl azide

: 87878-05-5
1-(3-hydroxy-4-carboxyphenyl)-4-carboxy-5-phenyl-1H-1,2,3-triazole

Guidance literature:: Multi-step reaction with 2 steps

1: 94 percent / methanol; diethyl ether / 0.17 h / Ambient temperature

2: 1.) sodium methoxyde, 2.) 2M NaOH / 1.) MeOH, r.t., 30 min; 50 deg C, 24 h, 2.) water, reflux, 60 min

With sodium hydroxide; sodium methylate; In methanol; diethyl ether;

Reference yield:

: 65-49-6
4-Aminosalicylic acid

: 87878-05-5
1-(3-hydroxy-4-carboxyphenyl)-4-carboxy-5-phenyl-1H-1,2,3-triazole

Guidance literature:: Multi-step reaction with 3 steps

1: 1.) 12M HCl, NaNO₂, 2.) NaN₃ / 1.) H₂O, 0 - 5 deg C, 20-30 min, 2.) H₂O

2: 94 percent / methanol; diethyl ether / 0.17 h / Ambient temperature

3: 1.) sodium methoxyde, 2.) 2M NaOH / 1.) MeOH, r.t., 30 min; 50 deg C, 24 h, 2.) water, reflux, 60 min

With hydrogenchloride; sodium hydroxide; sodium azide; sodium methylate; sodium nitrite; In methanol; diethyl ether;

Reference yield:

: 4136-97-4
methyl 4-aminosalicylate

: 87878-05-5
1-(3-hydroxy-4-carboxyphenyl)-4-carboxy-5-phenyl-1H-1,2,3-triazole

Guidance literature:: Multi-step reaction with 2 steps

1: 1.) 12M HCl, NaNO₂, 2.) NaN₃ / 1.) H₂O, 0 - 5 deg C, 15-20 min, 2.) H₂O, 10-14 deg C

2: 1.) sodium methoxyde, 2.) 2M NaOH / 1.) MeOH, r.t., 30 min; 50 deg C, 24 h, 2.) water, reflux, 60 min

With hydrogenchloride; sodium hydroxide; sodium azide; sodium methylate; sodium nitrite;