C₂₅H₂₇F₃O₅

Base Information

Chemical Name:C₂₅H₂₇F₃O₅
CAS No.:1427351-47-0
Molecular Formula:C₂₅H₂₇F₃O₅
Molecular Weight:464.482
Hs Code.:

C<sub>25</sub>H<sub>27</sub>F<sub>3</sub>O<sub>5</sub>

Synonyms:

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Chemical Property of C₂₅H₂₇F₃O₅

Chemical Property:

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Technology Process of C₂₅H₂₇F₃O₅

There total 9 articles about C₂₅H₂₇F₃O₅ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 20445-31-2
R-(+)-α-trifluoromethyl-α-methoxy-phenylacetic acid

: 1395345-59-1
C₁₅H₂₀O₃

: 1427351-47-0
C₂₅H₂₇F₃O₅

Guidance literature:: With dmap; 2,4,6-trichlorobenzoyl chloride; triethylamine; In toluene; at 0 - 23 ℃; for 3h; Inert atmosphere; Schlenk technique;
DOI:10.1039/c2ob26906f

Reference yield:

: 89238-99-3
O-(4-methoxybenzyl)-trichloroacetimidate

: 1427351-47-0
C₂₅H₂₇F₃O₅

Guidance literature:: Multi-step reaction with 9 steps

1.1: camphor-10-sulfonic acid / dichloromethane / 16 h / Inert atmosphere; Schlenk technique

2.1: diisobutylaluminium hydride / dichloromethane / 4.42 h / -78 °C / Inert atmosphere; Schlenk technique

3.1: Dess-Martin periodane / dichloromethane / 3 h / 0 - 23 °C / Inert atmosphere; Schlenk technique

4.1: diethylzinc / toluene / 1 h / Inert atmosphere; Schlenk technique; Reflux

4.2: 1 h / 23 °C / Inert atmosphere; Schlenk technique

4.3: Inert atmosphere; Schlenk technique

5.1: 2,6-dimethylpyridine / dichloromethane / 1 h / -78 °C / Inert atmosphere; Schlenk technique

6.1: potassium carbonate / methanol / 1 h / 23 °C / Inert atmosphere; Schlenk technique

7.1: diisobutylaluminium hydride; zirconocene dichloride; iodine / tetrahydrofuran / 1 h / -78 - 23 °C / Inert atmosphere; Schlenk technique

8.1: diethylzinc / toluene / 1 h / Inert atmosphere; Schlenk technique; Reflux

8.2: 1 h / 23 °C / Inert atmosphere; Schlenk technique

8.3: Inert atmosphere; Schlenk technique

9.1: triethylamine; 2,4,6-trichlorobenzoyl chloride; dmap / toluene / 3 h / 0 - 23 °C / Inert atmosphere; Schlenk technique

With 2,6-dimethylpyridine; dmap; zirconocene dichloride; 2,4,6-trichlorobenzoyl chloride; camphor-10-sulfonic acid; iodine; diethylzinc; diisobutylaluminium hydride; potassium carbonate; Dess-Martin periodane; triethylamine; In tetrahydrofuran; methanol; dichloromethane; toluene;
DOI:10.1039/c2ob26906f

Reference yield:

: 132969-71-2
methyl (2S)-[(4-methoxybenzyl)oxy]-2-methylpropanoate

: 1427351-47-0
C₂₅H₂₇F₃O₅

Guidance literature:: Multi-step reaction with 8 steps

1.1: diisobutylaluminium hydride / dichloromethane / 4.42 h / -78 °C / Inert atmosphere; Schlenk technique

2.1: Dess-Martin periodane / dichloromethane / 3 h / 0 - 23 °C / Inert atmosphere; Schlenk technique

3.1: diethylzinc / toluene / 1 h / Inert atmosphere; Schlenk technique; Reflux

3.2: 1 h / 23 °C / Inert atmosphere; Schlenk technique

3.3: Inert atmosphere; Schlenk technique

4.1: 2,6-dimethylpyridine / dichloromethane / 1 h / -78 °C / Inert atmosphere; Schlenk technique

5.1: potassium carbonate / methanol / 1 h / 23 °C / Inert atmosphere; Schlenk technique

6.1: diisobutylaluminium hydride; zirconocene dichloride; iodine / tetrahydrofuran / 1 h / -78 - 23 °C / Inert atmosphere; Schlenk technique

7.1: diethylzinc / toluene / 1 h / Inert atmosphere; Schlenk technique; Reflux

7.2: 1 h / 23 °C / Inert atmosphere; Schlenk technique

7.3: Inert atmosphere; Schlenk technique

8.1: triethylamine; 2,4,6-trichlorobenzoyl chloride; dmap / toluene / 3 h / 0 - 23 °C / Inert atmosphere; Schlenk technique

With 2,6-dimethylpyridine; dmap; zirconocene dichloride; 2,4,6-trichlorobenzoyl chloride; iodine; diethylzinc; diisobutylaluminium hydride; potassium carbonate; Dess-Martin periodane; triethylamine; In tetrahydrofuran; methanol; dichloromethane; toluene;
DOI:10.1039/c2ob26906f