1,3-bis(4-chlorobenzyl)-N-(4-methoxyphenyl)-1,3,2-diazaphosphinan-2-amine 2-oxide

Base Information

• Chemical Name: 1,3-bis(4-chlorobenzyl)-N-(4-methoxyphenyl)-1,3,2-diazaphosphinan-2-amine 2-oxide
• CAS No.: 1178-74-1
• Molecular Formula: C₂₄H₂₆Cl₂N₃O₂P
• Molecular Weight: 490.369
• Mol file: 1178-74-1.mol

Synonyms:1,3,2-Diazaphosphorine,2-p-anisidino-1,3-bis(p-chlorobenzyl)hexahydro-, 2-oxide (7CI,8CI); NSC 67644

Chemical Property of 1,3-bis(4-chlorobenzyl)-N-(4-methoxyphenyl)-1,3,2-diazaphosphinan-2-amine 2-oxide

Chemical Property:

• Vapor Pressure: 4.87E-15mmHg at 25°C
• Boiling Point: 614.6°C at 760 mmHg
• Flash Point: 325.5°C
• Density: 1.35g/cm³

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 1,3-bis(4-chlorobenzyl)-N-(4-methoxyphenyl)-1,3,2-diazaphosphinan-2-amine 2-oxide

There total 1 articles about 1,3-bis(4-chlorobenzyl)-N-(4-methoxyphenyl)-1,3,2-diazaphosphinan-2-amine 2-oxide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

N,N'-bis(4-chlorobenzyl)trimethylenediamine (59211-71-1) + N-4-methoxyphenylphosphoramidic dichloride (51250-37-4) → [1,3-bis-(4-chloro-benzyl)-2-oxo-2λ5-[1,3,2]diazaphosphinan-2-yl]-(4-methoxy-phenyl)-amine (1178-74-1)

Guidance literature:

In benzene;

DOI:10.1021/jm00326a030

upstream raw materials:

N,N'-bis(4-chlorobenzyl)trimethylenediamine

N-4-methoxyphenylphosphoramidic dichloride