TiCl₃NSi(CH₃)3P(C₆H₅)2CHC₆H₄C(CH₃)3

Base Information

Chemical Name:TiCl₃NSi(CH₃)3P(C₆H₅)2CHC₆H₄C(CH₃)3
CAS No.:344780-12-7
Molecular Formula:C₂₆H₃₃Cl₃NPSiTi
Molecular Weight:572.853
Hs Code.:

TiCl<sub>3</sub>NSi(CH<sub>3</sub>)3P(C<sub>6</sub>H<sub>5</sub>)2CHC<sub>6</sub>H<sub>4</sub>C(CH<sub>3</sub>)3

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Suppliers and Price of TiCl₃NSi(CH₃)3P(C₆H₅)2CHC₆H₄C(CH₃)3

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Chemical Property of TiCl₃NSi(CH₃)3P(C₆H₅)2CHC₆H₄C(CH₃)3

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Technology Process of TiCl₃NSi(CH₃)3P(C₆H₅)2CHC₆H₄C(CH₃)3

There total 2 articles about TiCl₃NSi(CH₃)3P(C₆H₅)2CHC₆H₄C(CH₃)3 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 84.0%

: 344780-11-6
(CH₃)3SiNP(C₆H₅)2CH₂C₆H₄C(CH₃)3

: 7550-45-0
titanium tetrachloride

: 344780-13-8
TiCl₃NP(C₆H₅)2CH₂C₆H₄C(CH₃)3

: 344780-12-7
TiCl₃NSi(CH₃)3P(C₆H₅)2CHC₆H₄C(CH₃)3

Guidance literature:: In toluene; byproducts: (CH3)3SiCl; (N2); addn. dropwise a soln. of TiCl4 in toluene to a soln. of ligand intoluene at -78°C over a period of 10 min, warming to room temp., stirring for 32 h; concn., addn. of light petroleum ether, drying in vac.; elem. anal.;
DOI:10.1039/b009082o

Reference yield: 48.0%

: 344780-11-6
(CH₃)3SiNP(C₆H₅)2CH₂C₆H₄C(CH₃)3

: 7550-45-0
titanium tetrachloride

: 344780-12-7
TiCl₃NSi(CH₃)3P(C₆H₅)2CHC₆H₄C(CH₃)3

Guidance literature:: With C₄H₉Li; In toluene; (N2); addn. of C4H9Li to a soln. of ligand in toluene at -78°C over a period of 10 min, warming to room temp., stirring for 2 h, addn. dropwise to a soln. of TiCl4 in toluene at -70°C, warming to room temp., stirring for 2 h; filtration, concn., addn. of light petroleum ether;
DOI:10.1039/b009082o