tetraphenylarsonium bis(cis-1,2-dicarbomethoxyethylenedithiolato)nickelate(III)

Base Information

Chemical Name:tetraphenylarsonium bis(cis-1,2-dicarbomethoxyethylenedithiolato)nickelate(III)
CAS No.:84914-02-3
Molecular Formula:C₁₂H₁₂NiO₈S₄*C₂₄H₂₀As
Molecular Weight:854.521
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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of tetraphenylarsonium bis(cis-1,2-dicarbomethoxyethylenedithiolato)nickelate(III)

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Technology Process of tetraphenylarsonium bis(cis-1,2-dicarbomethoxyethylenedithiolato)nickelate(III)

There total 1 articles about tetraphenylarsonium bis(cis-1,2-dicarbomethoxyethylenedithiolato)nickelate(III) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 56.0%

: nickel(II) chloride hexahydrate

: 73003-83-5
tetraphenylarsonium chloride hydrochloride

: 84914-02-3
tetraphenylarsonium bis(cis-1,2-dicarbomethoxyethylenedithiolato)nickelate(III)

Guidance literature:: With mercuric acetate; lithium methoxide; 4,5-dicarbomethoxy-1,3-dithiol-2-thion; In tetrahydrofuran; methanol; thion and solid mercuric acetate stirred rapidly in THF/methanol at room temp. for 24 h, filtered, LiOMe in methanol added to filtrate, NiCl2*6H2O in methanol added, solid Ph4AsCl*HCl added, allowed to stand at roomtemp. for 24 h; concd. in vac., product filtered, dried, recrystd. from warm acetone; elem. anal.;
DOI:10.1016/S0020-1693(00)88942-2