rac-ethylenebis((o-hydroxyphenyl)glycine) manganese(III) complex sodium salt*1.5H₂O

Base Information

• Chemical Name: rac-ethylenebis((o-hydroxyphenyl)glycine) manganese(III) complex sodium salt*1.5H₂O
• CAS No.: 81654-79-7
• Molecular Formula: C₁₈H₁₆N₂O₆*H₂O*Mn*Na
• Molecular Weight: 461.286
• Mol file: 81654-79-7.mol

Synonyms:

Chemical Property of rac-ethylenebis((o-hydroxyphenyl)glycine) manganese(III) complex sodium salt*1.5H₂O

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of rac-ethylenebis((o-hydroxyphenyl)glycine) manganese(III) complex sodium salt*1.5H₂O

There total 2 articles about rac-ethylenebis((o-hydroxyphenyl)glycine) manganese(III) complex sodium salt*1.5H₂O which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

manganese triacetate (638-38-0,993-02-2,2180-18-9,15411-95-7,22981-23-3,27004-39-3) + rac-N,N'-Ethylenebis<2-(o-hydroxyphenyl)glycine> (1170-02-1,81944-53-8,81944-54-9) → rac-ethylenebis((o-hydroxyphenyl)glycine) manganese(III) complex sodium salt*1.5H2O (81654-79-7)

Guidance literature:

With NaOH; In water; ligand was treated with NaOH and Mn compd. (N2); stirring overnight; filtration, evapn., recrystn. from aq. EtOH; elem. anal.;

DOI:10.1021/ic00138a012

Reference yield:

rac-N,N'-Ethylenebis<2-(o-hydroxyphenyl)glycine> (1170-02-1,81944-53-8,81944-54-9) + manganese(ll) chloride (7773-01-5) → rac-ethylenebis((o-hydroxyphenyl)glycine) manganese(III) complex sodium salt*1.5H2O (81654-79-7)

Guidance literature:

With NaOH; air; In water; ligand was treated with NaOH and Mn compd.; stirring overnight; filtration, evapn., recrystn. from aq. EtOH; elem. anal.;

DOI:10.1021/ic00138a012

upstream raw materials:

manganese triacetate

rac-N,N'-Ethylenebis<2-(o-hydroxyphenyl)glycine>

manganese(ll) chloride

Refernces