chloro(N,N'-bis(2,6-diisopropylphenyl)(tert-butyl)amidinato)tin(II)

Base Information

Chemical Name:chloro(N,N'-bis(2,6-diisopropylphenyl)(tert-butyl)amidinato)tin(II)
CAS No.:958298-92-5
Molecular Formula:C₂₉H₄₃ClN₂Sn
Molecular Weight:573.837
Hs Code.:

Synonyms:

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Chemical Property of chloro(N,N'-bis(2,6-diisopropylphenyl)(tert-butyl)amidinato)tin(II)

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Technology Process of chloro(N,N'-bis(2,6-diisopropylphenyl)(tert-butyl)amidinato)tin(II)

There total 1 articles about chloro(N,N'-bis(2,6-diisopropylphenyl)(tert-butyl)amidinato)tin(II) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 69.0%

: tin(ll) chloride

: 630111-11-4,865200-87-9,1256380-68-3
N,N'-bis(2,6-diisopropylphenyl)(tert-butyl)amidine

: 958298-92-5
chloro(N,N'-bis(2,6-diisopropylphenyl)(tert-butyl)amidinato)tin(II)

Guidance literature:: With n-BuLi; In hexane; toluene; suspn. of t-BuC(NC6H3-2,6-i-Pr2)2Li in toluene (formed in situ from n-BuLi in hexanes and tert-butylamidine) added to SnCl2 in toluene at -78°C; warmed to room temp.; stirred for 18 h; soln. filtered; volatiles removed; solid recrystd. from heptane; elem. anal.;
DOI:10.1039/b706663e

Reference yield: 66.0%

: 958298-92-5
chloro(N,N'-bis(2,6-diisopropylphenyl)(tert-butyl)amidinato)tin(II)

: 4039-32-1
lithium hexamethyldisilazane

: 958298-95-8
(N,N'-bis(2,6-diisopropylphenyl)(tert-butyl)amidinato)tin(II)(N(SiMe₃)2)

Guidance literature:: In toluene; suspn. of LiN(SiMe3)2 in toluene added dropwise to soln. of Sn complex in toluene at -78°C; stirred for 18 h upon warming to room temp.; filtered; filtrate concd. under reduced pressure; solid recrystd. from satd. heptane soln. at -30°C; elem. anal.;
DOI:10.1039/b706663e

Reference yield: 57.0%

: 958298-92-5
chloro(N,N'-bis(2,6-diisopropylphenyl)(tert-butyl)amidinato)tin(II)

: 3585-33-9
lithium dimethylamide

: 958298-94-7
(N,N'-bis(2,6-diisopropylphenyl)(tert-butyl)amidinato)tin(II)(NMe₂)

Guidance literature:: In toluene; suspn. of LiNMe2 in toluene added dropwise to soln. of Sn complex in toluene at -78°C; stirred for 18 h upon warming to room temp.; filtered; filtrate concd. under reduced pressure; solid recrystd. from satd. heptane soln. at -30°C; elem. anal.;
DOI:10.1039/b706663e