[(C₅H₅)(CO)(P(C₆H₅)3)Fe(C₄H₈O)]⁽¹⁺⁾*O₃SCF₃^(1-)=[(C₅H₅)(CO)(P(C₆H₅)3)Fe(C₄H₈O)](O₃SCF₃)

Base Information

• Chemical Name: [(C₅H₅)(CO)(P(C₆H₅)3)Fe(C₄H₈O)]⁽¹⁺⁾*O₃SCF₃^(1-)=[(C₅H₅)(CO)(P(C₆H₅)3)Fe(C₄H₈O)](O₃SCF₃)
• CAS No.: 463945-72-4
• Molecular Formula: CF₃O₃S*C₂₈H₂₈FeO₂P
• Molecular Weight: 632.42

Synonyms:

Chemical Property of [(C₅H₅)(CO)(P(C₆H₅)3)Fe(C₄H₈O)]⁽¹⁺⁾*O₃SCF₃^(1-)=[(C₅H₅)(CO)(P(C₆H₅)3)Fe(C₄H₈O)](O₃SCF₃)

Chemical Property:

Purity/Quality:

Safty Information:

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MSDS Files:

Useful:

Technology Process of [(C₅H₅)(CO)(P(C₆H₅)3)Fe(C₄H₈O)]⁽¹⁺⁾*O₃SCF₃^(1-)=[(C₅H₅)(CO)(P(C₆H₅)3)Fe(C₄H₈O)](O₃SCF₃)

There total 1 articles about [(C₅H₅)(CO)(P(C₆H₅)3)Fe(C₄H₈O)]⁽¹⁺⁾*O₃SCF₃^(1-)=[(C₅H₅)(CO)(P(C₆H₅)3)Fe(C₄H₈O)](O₃SCF₃) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

tetrahydrofuran (109-99-9,24979-97-3,77392-70-2) + cyclopentadienyl iron carbonyl triphenylphosphine iodide + silver trifluoromethanesulfonate (2923-28-6) → [(C5H5)(CO)(P(C6H5)3)Fe(C4H8O)](1+)*O3SCF3(1-)=[(C5H5)(CO)(P(C6H5)3)Fe(C4H8O)](O3SCF3) (463945-72-4)

Guidance literature:

In tetrahydrofuran; Ar; react. of iodide with stoich. amt. of silver salt in THF soln. at room temp.; filtration over Celite, evapn. to dryness;

DOI:10.1021/om020283z

Reference yield: 70.0%

Na[W(CO)5CN] + [(C5H5)(CO)(P(C6H5)3)Fe(C4H8O)](1+)*O3SCF3(1-)=[(C5H5)(CO)(P(C6H5)3)Fe(C4H8O)](O3SCF3) (463945-72-4) → [(C5H5)(CO)(P(C6H5)3)FeNCW(CO)5]

Guidance literature:

In dichloromethane; byproducts: NaO3SCF3; (Ar); standard Schlenk technique; soln. of Fe complex in CH2Cl2 was added to suspn. of W complex in CH2Cl2; mixt. was stirred at -30°C for 1 h; filtered through Celite; evapd. (vac.); chromd. (alumina, petroleum ether/CH2Cl2, 2/1); elem. anal.;

DOI:10.1016/j.jorganchem.2004.04.021

Reference yield: 62.0%

Na(1+)*Mo(CN)(CO)5(1-) = Na[Mo(CN)(CO)5] + [(C5H5)(CO)(P(C6H5)3)Fe(C4H8O)](1+)*O3SCF3(1-)=[(C5H5)(CO)(P(C6H5)3)Fe(C4H8O)](O3SCF3) (463945-72-4) + acetonitrile (75-05-8,26809-02-9) → [(C5H5)(CO)(P(C6H5)3)Fe(NCCH3)](1+)*[NCMo(CO)5](1-)=[(C5H5)(CO)(P(C6H5)3)Fe(NCCH3)][NCMo(CO)5] (743422-09-5)

Guidance literature:

In acetone; acetonitrile; (Ar); standard Schlenk technique; soln. of Fe complex in acetone was added dropwise to stirred suspn. of Mo complex in CH3CN; mixt. was maintained at -30°C for 2 h; warmed to room temp.; filtered through Celite; evapd.; chromd. (alumina, CH2Cl2; CH3CN); crystd. from CH2Cl2 soln. layered with Et2O at -5°C; elem. anal.;

DOI:10.1016/j.jorganchem.2004.04.021

upstream raw materials:

tetrahydrofuran

silver trifluoromethanesulfonate

Downstream raw materials:

[(C₅H₅)(CO)2Fe(N₄CC₆H₄CN)Fe(CO)(P(C₆H₅)3)(C₅H₅)]⁽¹⁺⁾*O₃SCF₃^(1-)=[(C₅H₅)(CO)2Fe(N₄CC₆H₄CN)Fe(CO)(P(C₆H₅)3)(C₅H₅)]O₃SCF₃

[(C₅H₅)(CO)(P(OCH₃)3)FeN₄CC₆H₄CNFe(CO)(P(C₆H₅)3)(C₅H₅)]⁽¹⁺⁾*O₃SCF₃^(1-)=[C₈H₄N₅(Fe(CO)(C₅H₅))2(P(OCH₃)3)(P(C₆H₅)3)]O₃SCF₃

[(C₅H₅)(CO)(P(C₆H₅)3)Fe(N₄CC₆H₄CN)]

[(C₅H₅)(CO)(P(C₆H₅)3)Fe(NCCH₃)]⁽¹⁺⁾*[NCMo(CO)5]^(1-)=[(C₅H₅)(CO)(P(C₆H₅)3)Fe(NCCH₃)][NCMo(CO)5]

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