Technology Process of μ2,η1-N-[(N,N-dimethylamino)dimethylsilyl]-2,6-diisopropylanilidohafnium chloride-lithium chloride Et2O adduct
There total 1 articles about μ2,η1-N-[(N,N-dimethylamino)dimethylsilyl]-2,6-diisopropylanilidohafnium chloride-lithium chloride Et2O adduct which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
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In
tetrahydrofuran;
(Ar); std. Schlenk technique; HfCl4 (1 equiv.) was added to soln. of Li compd. (2 equiv.) in THF at -78°C; stirred while warmed to room temp.; stirred for 24 h; evapd. (vac.); extd. (toluene); filtered; dried (vac.); dissolved in ether; crystd.; elem. anal.;
DOI:10.1021/om100044b
