(+/-)-cis-4'-acetylkhellactone

Base Information

Chemical Name:(+/-)-cis-4'-acetylkhellactone
CAS No.:4955-21-9
Molecular Formula:C₁₆H₁₆O₆
Molecular Weight:304.299
Hs Code.:

Synonyms:

Suppliers and Price of (+/-)-cis-4'-acetylkhellactone

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (+/-)-cis-4'-acetylkhellactone

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of (+/-)-cis-4'-acetylkhellactone

There total 6 articles about (+/-)-cis-4'-acetylkhellactone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 523-59-1
seseline

: 4955-21-9,35345-45-0,107080-28-4,112346-42-6,118492-19-6,118492-23-2
(+/-)-cis-4'-acetylkhellactone

Guidance literature:: Multi-step reaction with 2 steps

1: 75 percent Turnov_. / OsO₄, N-methylmorpholine-N-oxide dihydrate / 2-methyl-propan-2-ol; tetrahydrofuran; H₂O / 72 h / Ambient temperature

2: 65 percent Turnov_. / BF₃*Et₂O / tetrahydrofuran / 2.8 h / Ambient temperature

With osmium(VIII) oxide; boron trifluoride diethyl etherate; 4-methylmorpholine N-oxide; In tetrahydrofuran; water; tert-butyl alcohol;
DOI:10.3987/R-1987-05-1239

Reference yield:

: 523-59-1
seseline

: 152615-14-0
qianhucomarin B

: 4955-21-9,35345-45-0,107080-28-4,112346-42-6,118492-19-6,118492-23-2
(+/-)-cis-4'-acetylkhellactone

Guidance literature:: Multi-step reaction with 2 steps

1: 4-methylmorpholine N-oxide; osmium(VIII) oxide; water / acetone / 24 h / 20 °C

2: dimethyltin dichloride; potassium carbonate / tetrahydrofuran / 24 h / 0 °C

With osmium(VIII) oxide; water; dimethyltin dichloride; potassium carbonate; 4-methylmorpholine N-oxide; In tetrahydrofuran; acetone;

Reference yield:

: 523-59-1
seseline

: 64-19-7,77671-22-8
acetic acid

: 4955-21-9,35345-45-0,107080-28-4,112346-42-6,118492-19-6,118492-23-2
(+/-)-trans-4'-acetylkhellactone

Guidance literature:: With water; iodine; silver(I) acetate; Yield given. Multistep reaction; 1.) 30 min, 2.) from 95 to 100 deg C, 2 5 h;
DOI:10.3987/R-1987-05-1239