Technology Process of C43H55N3O15S3
There total 7 articles about C43H55N3O15S3 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
Multi-step reaction with 6 steps
1: 83 percent / m-chloroperbenzoic acid / CHCl3 / 1 h / 20 °C
2: 75 percent / iPr2EtN / acetone / 0.17 h / 40 °C
3: 41 percent / tetrahydrofuran / 0.5 h / 60 °C
4: pyridine / 2.5 h / 20 °C
5: 85 percent / dimethylsulfoxide / 18 h / 80 °C
6: 1.)OsO4; 2.) NaIO4 / 1.) aq. dioxan, 20 deg C, 0.5 h; 2.) 1.5 h
With
sodium periodate; osmium(VIII) oxide; N-ethyl-N,N-diisopropylamine; 3-chloro-benzenecarboperoxoic acid;
In
tetrahydrofuran; pyridine; chloroform; dimethyl sulfoxide; acetone;
- Guidance literature:
-
Multi-step reaction with 2 steps
1: 85 percent / dimethylsulfoxide / 18 h / 80 °C
2: 1.)OsO4; 2.) NaIO4 / 1.) aq. dioxan, 20 deg C, 0.5 h; 2.) 1.5 h
With
sodium periodate; osmium(VIII) oxide;
In
dimethyl sulfoxide;
- Guidance literature:
-
Multi-step reaction with 7 steps
2: 83 percent / m-chloroperbenzoic acid / CHCl3 / 1 h / 20 °C
3: 75 percent / iPr2EtN / acetone / 0.17 h / 40 °C
4: 41 percent / tetrahydrofuran / 0.5 h / 60 °C
5: pyridine / 2.5 h / 20 °C
6: 85 percent / dimethylsulfoxide / 18 h / 80 °C
7: 1.)OsO4; 2.) NaIO4 / 1.) aq. dioxan, 20 deg C, 0.5 h; 2.) 1.5 h
With
sodium periodate; osmium(VIII) oxide; N-ethyl-N,N-diisopropylamine; 3-chloro-benzenecarboperoxoic acid;
In
tetrahydrofuran; pyridine; chloroform; dimethyl sulfoxide; acetone;