6'-N-(benzyloxycarbonyl)-3',4':5,6-di-O-cyclohexylidene-1,2',3-tri-N-tosylneamine

Base Information

Chemical Name:6'-N-(benzyloxycarbonyl)-3',4':5,6-di-O-cyclohexylidene-1,2',3-tri-N-tosylneamine
CAS No.:88985-60-8
Molecular Formula:C₅₃H₆₆N₄O₁₄S₃
Molecular Weight:1079.32
Hs Code.:

Synonyms:6'-N-(benzyloxycarbonyl)-3',4':5,6-di-O-cyclohexylidene-1,2',3-tri-N-tosylneamine

Suppliers and Price of 6'-N-(benzyloxycarbonyl)-3',4':5,6-di-O-cyclohexylidene-1,2',3-tri-N-tosylneamine

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 6'-N-(benzyloxycarbonyl)-3',4':5,6-di-O-cyclohexylidene-1,2',3-tri-N-tosylneamine

Chemical Property:

Purity/Quality:: 98% ^*data from raw suppliers

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Technology Process of 6'-N-(benzyloxycarbonyl)-3',4':5,6-di-O-cyclohexylidene-1,2',3-tri-N-tosylneamine

There total 5 articles about 6'-N-(benzyloxycarbonyl)-3',4':5,6-di-O-cyclohexylidene-1,2',3-tri-N-tosylneamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 933-40-4
cycloxexanone dimethyl ketal

: [(2R,3S,4R,5R,6R)-6-[(1R,2R,3S,4R,6S)-2,3-Dihydroxy-4,6-bis-(toluene-4-sulfonylamino)-cyclohexyloxy]-3,4-dihydroxy-5-(toluene-4-sulfonylamino)-tetrahydro-pyran-2-ylmethyl]-carbamic acid benzyl ester

: 88985-60-8
6'-N-(benzyloxycarbonyl)-3',4':5,6-di-O-cyclohexylidene-1,2',3-tri-N-tosylneamine

Guidance literature:: With toluene-4-sulfonic acid; In N,N-dimethyl-formamide; at 50 ℃; for 72h; under 25 Torr;
DOI:10.1246/bcsj.57.529

Reference yield:

: 3947-65-7
neomycin A

: 88985-60-8
6'-N-(benzyloxycarbonyl)-3',4':5,6-di-O-cyclohexylidene-1,2',3-tri-N-tosylneamine

Guidance literature:: Multi-step reaction with 3 steps

1: triethylamine / methanol; H₂O / 5 h / Ambient temperature

2: 166 g / Na₂CO₃ / H₂O; dioxane / 5 h / Ambient temperature

3: 132.2 g / TsOH / dimethylformamide / 72 h / 50 °C / 25 Torr

With sodium carbonate; toluene-4-sulfonic acid; triethylamine; In 1,4-dioxane; methanol; water; N,N-dimethyl-formamide;
DOI:10.1246/bcsj.57.529

Reference yield:

: N-<(benzyloxy)carbonyl>-5-norbornene-2,3-dicarboximide

: 88985-60-8
6'-N-(benzyloxycarbonyl)-3',4':5,6-di-O-cyclohexylidene-1,2',3-tri-N-tosylneamine

Guidance literature:: Multi-step reaction with 3 steps

1: triethylamine / methanol; H₂O / 5 h / Ambient temperature

2: 166 g / Na₂CO₃ / H₂O; dioxane / 5 h / Ambient temperature

3: 132.2 g / TsOH / dimethylformamide / 72 h / 50 °C / 25 Torr

With sodium carbonate; toluene-4-sulfonic acid; triethylamine; In 1,4-dioxane; methanol; water; N,N-dimethyl-formamide;
DOI:10.1246/bcsj.57.529