NiI₂((C₆H₅)2PCH₂SC₆H₅)2

Base Information

• Chemical Name: NiI₂((C₆H₅)2PCH₂SC₆H₅)2
• CAS No.: 82287-74-9
• Molecular Formula: C₃₈H₃₄I₂NiP₂S₂
• Molecular Weight: 929.266

Synonyms:

Chemical Property of NiI₂((C₆H₅)2PCH₂SC₆H₅)2

Chemical Property:

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Technology Process of NiI₂((C₆H₅)2PCH₂SC₆H₅)2

There total 1 articles about NiI₂((C₆H₅)2PCH₂SC₆H₅)2 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 47.0%

nickel(II) nitrate hexahydrate + (diphenylphosphanyl)(thiophenyl)methane (82270-61-9) → NiI2((C6H5)2PCH2SC6H5)2 (82287-74-9)

Guidance literature:

With KI; In chloroform; butan-1-ol; byproducts: H2O, KNO3; (N2), Ni-salt and KI refluxed for 2 h in n-butanol, filtered, treated with a soln. of the org. compd. in warm CHCl3 in the warmth; CHCl3 removed in vacuo, cooled, stored at -15°C, filtered off, washed with n-butanol, dried in high vacuo at room temp., elem. anal.;

upstream raw materials:

(diphenylphosphanyl)(thiophenyl)methane

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