(C₆H₁₁)Cl₂PMn(C₅H₅)(CO)2

Base Information

Chemical Name:(C₆H₁₁)Cl₂PMn(C₅H₅)(CO)2
CAS No.:95608-75-6
Molecular Formula:C₁₃H₁₆Cl₂MnO₂P
Molecular Weight:361.087
Hs Code.:

(C<sub>6</sub>H<sub>11</sub>)Cl<sub>2</sub>PMn(C<sub>5</sub>H<sub>5</sub>)(CO)2

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Chemical Property of (C₆H₁₁)Cl₂PMn(C₅H₅)(CO)2

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Technology Process of (C₆H₁₁)Cl₂PMn(C₅H₅)(CO)2

There total 1 articles about (C₆H₁₁)Cl₂PMn(C₅H₅)(CO)2 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 56.0%

: dicarbonyl(η(5)-cyclopentadienyl)manganese(THF)

: 2844-89-5
dichlorocyclohexylphosphine

: 95608-75-6
(C₆H₁₁)Cl₂PMn(C₅H₅)(CO)2

Guidance literature:: In tetrahydrofuran; addn. of the dichlorophosphane to soln. of (THF)MnCp(CO)2 (under N2), stirred (20 h); evapn. (high vac.), addn. of n-pentane, cooled (-78°C), decanted, sublimation of excess MnCp(CO)3, addn. of toluene, filtered (silicagel), evapn., addn. of n-pentane, cooled (-78°C)., dried (high vac.,20°C); elem. anal.;

Reference yield: 80.0%

: 95608-75-6
(C₆H₁₁)Cl₂PMn(C₅H₅)(CO)2

: 917-54-4
methyllithium

: 95608-86-9
(C₆H₁₁)(CH₃)2PMn(C₅H₅)(CO)2

Guidance literature:: With N,N,N',N'-tetramethylethylene diamine; In tetrahydrofuran; pentane; byproducts: LiCl; addn. of CH3Li in pentane in presence of TMEDA to soln. of the Mn compd. in THF (N2, -78°C), allowed to warm to 25°C; evapn. (E-3 mbar), chromy. (silicagel, n-pentane/ toluene (1:3), -25°C), crystn. on trituration with pentane, recrystn. (n-pentane); elem. anal.;

Reference yield: 66.0%

: 95608-75-6
(C₆H₁₁)Cl₂PMn(C₅H₅)(CO)2

: 95608-88-1
(C₆H₁₁)(CH₃(CH₂)3)2PMn(C₅H₅)(CO)2

Guidance literature:: With N,N,N',N'-tetramethylethylene diamine; n-C₄H₉Li; In tetrahydrofuran; pentane; byproducts: LiCl; addn. of n-butylLi in pentane in presence of TMEDA to soln. of the Mn compd. in THF (N2, -78°C), allowed to warm to 25°C; evapn. (E-3 mbar), chromy. (silicagel, n-pentane/ toluene (1:2), -25°C), crystn. on trituration with pentane, recrystn. (n-pentane); elem. anal.;