(11-Hydroxy-undecyl)-methylphenylphosphinoxid

Base Information

• Chemical Name: (11-Hydroxy-undecyl)-methylphenylphosphinoxid
• CAS No.: 19097-48-4
• Molecular Formula: C₁₈H₃₁O₂P
• Molecular Weight: 310.417
• Mol file: 19097-48-4.mol

Synonyms:

Chemical Property of (11-Hydroxy-undecyl)-methylphenylphosphinoxid

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of (11-Hydroxy-undecyl)-methylphenylphosphinoxid

There total 4 articles about (11-Hydroxy-undecyl)-methylphenylphosphinoxid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

1-Bromo-11-hydroxyundecane (1611-56-9) → (11-Hydroxy-undecyl)-methylphenylphosphinoxid (19097-48-4)

Guidance literature:

Multi-step reaction with 3 steps

1: ethanol / Heating

2: NaH / 0.75 h / 120 - 140 °C

3: (i) EtOH, (ii) aq. KOH

With sodium hydride; In ethanol;

DOI:10.1039/j39680001331

Reference yield:

triphenylphosphine (603-35-0) → (11-Hydroxy-undecyl)-methylphenylphosphinoxid (19097-48-4)

Guidance literature:

Multi-step reaction with 3 steps

1: ethanol / Heating

2: NaH / 0.75 h / 120 - 140 °C

3: (i) EtOH, (ii) aq. KOH

With sodium hydride; In ethanol;

DOI:10.1039/j39680001331

Reference yield:

(11?hydroxyundecyl)triphenylphosphonium bromide (19101-00-9) → (11-Hydroxy-undecyl)-methylphenylphosphinoxid (19097-48-4)

Guidance literature:

Multi-step reaction with 2 steps

1: NaH / 0.75 h / 120 - 140 °C

2: (i) EtOH, (ii) aq. KOH

With sodium hydride;

DOI:10.1039/j39680001331

upstream raw materials:

(11-Hydroxyundecyl)-diphenylphosphin

methyl iodide

1-Bromo-11-hydroxyundecane

(11?hydroxyundecyl)triphenylphosphonium bromide