[Co(BH₄)((C₆H₅)2P(CH₂)5P(C₆H₅)2)]2*0.5C₆H₆

Base Information

• Chemical Name: [Co(BH₄)((C₆H₅)2P(CH₂)5P(C₆H₅)2)]2*0.5C₆H₆
• CAS No.: 98482-12-3
• Molecular Formula: 0C₆H₆*C₅₈H₆₈B₂Co₂P₄
• Molecular Weight: 1067.74
• Mol file: 98482-12-3.mol

Synonyms:

Chemical Property of [Co(BH₄)((C₆H₅)2P(CH₂)5P(C₆H₅)2)]2*0.5C₆H₆

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
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MSDS Files:

Useful:

Technology Process of [Co(BH₄)((C₆H₅)2P(CH₂)5P(C₆H₅)2)]2*0.5C₆H₆

There total 1 articles about [Co(BH₄)((C₆H₅)2P(CH₂)5P(C₆H₅)2)]2*0.5C₆H₆ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

sodium tetrahydroborate (16940-66-2) + cobalt(II) chloride hexahydrate + 1,5-bis-(diphenylphosphino)pentane (27721-02-4) → [Co(BH4)((C6H5)2P(CH2)5P(C6H5)2)]2*0.5C6H6 (98482-12-3)

Guidance literature:

With NaBH₄; In ethanol; toluene; dropwise addn. of 4.5mmol NaBH4 in 5ml ethanol to a soln. of 2.37mmol CoCl2*6H2O and 6.79mmol phosphine in ethanol (18ml) and toluene (14ml) atroom temp.; performed under N2;; the ppt. was filtered off and washed through the filter with C6H6; the benzene washings were combined with the original filtrate; addn. of ethanol; crystn. at 0°C after 24h, recrystn. from C6H6/hexane (1:1); elem. anal.;;

upstream raw materials:

sodium tetrahydroborate

1,5-bis-(diphenylphosphino)pentane