(2S,3R,4S)-4-{(2S,5R)-5-[(R)-1-(2,6-Di-tert-butyl-4-methoxy-phenoxycarbonyl)-ethyl]-tetrahydro-furan-2-yl}-3-hydroxy-2-methyl-pentanoic acid methyl ester

Base Information

• Chemical Name: (2S,3R,4S)-4-{(2S,5R)-5-[(R)-1-(2,6-Di-tert-butyl-4-methoxy-phenoxycarbonyl)-ethyl]-tetrahydro-furan-2-yl}-3-hydroxy-2-methyl-pentanoic acid methyl ester
• CAS No.: 164413-26-7
• Molecular Formula: C₂₉H₄₆O₇
• Molecular Weight: 506.68

Synonyms:

Chemical Property of (2S,3R,4S)-4-{(2S,5R)-5-[(R)-1-(2,6-Di-tert-butyl-4-methoxy-phenoxycarbonyl)-ethyl]-tetrahydro-furan-2-yl}-3-hydroxy-2-methyl-pentanoic acid methyl ester

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
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MSDS Files:

Useful:

Technology Process of (2S,3R,4S)-4-{(2S,5R)-5-[(R)-1-(2,6-Di-tert-butyl-4-methoxy-phenoxycarbonyl)-ethyl]-tetrahydro-furan-2-yl}-3-hydroxy-2-methyl-pentanoic acid methyl ester

There total 1 articles about (2S,3R,4S)-4-{(2S,5R)-5-[(R)-1-(2,6-Di-tert-butyl-4-methoxy-phenoxycarbonyl)-ethyl]-tetrahydro-furan-2-yl}-3-hydroxy-2-methyl-pentanoic acid methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

sodium methylate (124-41-4) + (R)-2-{(2R,5S)-5-[(1S,2R,3S)-4-((S)-4-Benzyl-2-oxo-oxazolidin-3-yl)-2-hydroxy-1,3-dimethyl-4-oxo-butyl]-tetrahydro-furan-2-yl}-propionic acid 2,6-di-tert-butyl-4-methoxy-phenyl ester → (2S,3R,4S)-4-{(2S,5R)-5-[(R)-1-(2,6-Di-tert-butyl-4-methoxy-phenoxycarbonyl)-ethyl]-tetrahydro-furan-2-yl}-3-hydroxy-2-methyl-pentanoic acid methyl ester (164413-26-7)

Guidance literature:

Yield given;

DOI:10.1016/0040-4039(95)00471-N

Reference yield: 98.0%

t-butyldimethylsiyl triflate (69739-34-0) + (2S,3R,4S)-4-{(2S,5R)-5-[(R)-1-(2,6-Di-tert-butyl-4-methoxy-phenoxycarbonyl)-ethyl]-tetrahydro-furan-2-yl}-3-hydroxy-2-methyl-pentanoic acid methyl ester (164413-26-7) → (2S,3R,4R)-3-(tert-Butyl-dimethyl-silanyloxy)-4-{(2S,5R)-5-[(R)-1-(2,6-di-tert-butyl-4-methoxy-phenoxycarbonyl)-ethyl]-tetrahydro-furan-2-yl}-2-methyl-pentanoic acid methyl ester

Guidance literature:

DOI:10.1016/0040-4039(95)00471-N

upstream raw materials:

sodium methylate

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