benzhydrylbis(trimethylsilylmethyl)bis(tetrahydrofuran)lutetium

Base Information

Chemical Name:benzhydrylbis(trimethylsilylmethyl)bis(tetrahydrofuran)lutetium
CAS No.:889447-35-2
Molecular Formula:C₂₉H₄₉LuO₂Si₂
Molecular Weight:660.845
Hs Code.:

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Chemical Property of benzhydrylbis(trimethylsilylmethyl)bis(tetrahydrofuran)lutetium

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Technology Process of benzhydrylbis(trimethylsilylmethyl)bis(tetrahydrofuran)lutetium

There total 1 articles about benzhydrylbis(trimethylsilylmethyl)bis(tetrahydrofuran)lutetium which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 32.0%

: 10060-17-0
diphenylmethylpotassium

: 24614-69-5,144491-06-5,120496-88-0
LuCl₃(THF)3

: 1822-00-0
trimethylsilylmethyllithium

: 889447-35-2
benzhydrylbis(trimethylsilylmethyl)bis(tetrahydrofuran)lutetium

Guidance literature:: In tetrahydrofuran; diethyl ether; pentane; byproducts: LiCl, KCl; soln. of LiCH2SiMe3 in pentane added dropwise to stirred suspn. of Lu complex in THF-pentane-Et2O; stirred for 2 h; cooled to 0°C; soln. of KCHPh2 in THF added; stirred for 30 min; filtered; solvent evapd. in vac.; extd. with cold pentane; filtered extract slowly concd. in vac. at room temp.; pptd. on cooling to -78°C; elem. anal.;
DOI:10.1021/om0601201