Diisopropyl-phosphoramidous acid (2R,3S,5R)-2-[bis-(4-methoxy-phenyl)-phenyl-methoxymethyl]-5-(5-methyl-2,4-dioxo-3,4-dihydro-2H-pyrimidin-1-yl)-tetrahydro-furan-3-yl ester 2-triethylsilanyl-ethyl ester

Base Information

Chemical Name:Diisopropyl-phosphoramidous acid (2R,3S,5R)-2-[bis-(4-methoxy-phenyl)-phenyl-methoxymethyl]-5-(5-methyl-2,4-dioxo-3,4-dihydro-2H-pyrimidin-1-yl)-tetrahydro-furan-3-yl ester 2-triethylsilanyl-ethyl ester
CAS No.:173440-24-9
Molecular Formula:C₄₅H₆₄N₃O₈PSi
Molecular Weight:834.078
Hs Code.:

Diisopropyl-phosphoramidous acid (2R,3S,5R)-2-[bis-(4-methoxy-phenyl)-phenyl-methoxymethyl]-5-(5-methyl-2,4-dioxo-3,4-dihydro-2H-pyrimidin-1-yl)-tetrahydro-furan-3-yl ester 2-triethylsilanyl-ethyl ester

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Chemical Property of Diisopropyl-phosphoramidous acid (2R,3S,5R)-2-[bis-(4-methoxy-phenyl)-phenyl-methoxymethyl]-5-(5-methyl-2,4-dioxo-3,4-dihydro-2H-pyrimidin-1-yl)-tetrahydro-furan-3-yl ester 2-triethylsilanyl-ethyl ester

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Technology Process of Diisopropyl-phosphoramidous acid (2R,3S,5R)-2-[bis-(4-methoxy-phenyl)-phenyl-methoxymethyl]-5-(5-methyl-2,4-dioxo-3,4-dihydro-2H-pyrimidin-1-yl)-tetrahydro-furan-3-yl ester 2-triethylsilanyl-ethyl ester

There total 3 articles about Diisopropyl-phosphoramidous acid (2R,3S,5R)-2-[bis-(4-methoxy-phenyl)-phenyl-methoxymethyl]-5-(5-methyl-2,4-dioxo-3,4-dihydro-2H-pyrimidin-1-yl)-tetrahydro-furan-3-yl ester 2-triethylsilanyl-ethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 2916-67-8
2-(triethylsilyl)ethanol

: 173440-24-9,173440-39-6
Diisopropyl-phosphoramidous acid (2R,3S,5R)-2-[bis-(4-methoxy-phenyl)-phenyl-methoxymethyl]-5-(5-methyl-2,4-dioxo-3,4-dihydro-2H-pyrimidin-1-yl)-tetrahydro-furan-3-yl ester 2-triethylsilanyl-ethyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: PCl₃ / diethyl ether / 2 h / Ambient temperature

2: diethyl ether / 24 h / Ambient temperature

3: 1.) 1H-tetrazol, 1.) Et₃N / 1.) MeCN, 20 min; 3 h, 2.) -20 deg C, 12 h

With 1H-tetrazole; triethylamine; phosphorus trichloride; In diethyl ether;

Reference yield:

: C₈H₁₉Cl₂OPSi

: 173440-24-9,173440-39-6
Diisopropyl-phosphoramidous acid (2R,3S,5R)-2-[bis-(4-methoxy-phenyl)-phenyl-methoxymethyl]-5-(5-methyl-2,4-dioxo-3,4-dihydro-2H-pyrimidin-1-yl)-tetrahydro-furan-3-yl ester 2-triethylsilanyl-ethyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: diethyl ether / 24 h / Ambient temperature

2: 1.) 1H-tetrazol, 1.) Et₃N / 1.) MeCN, 20 min; 3 h, 2.) -20 deg C, 12 h

With 1H-tetrazole; triethylamine; In diethyl ether;