2,4-Di-O-Acetyl-1,3-O-benzyliden-α-D-tagatopyranose

Base Information

Chemical Name:2,4-Di-O-Acetyl-1,3-O-benzyliden-α-D-tagatopyranose
CAS No.:77387-31-6
Molecular Formula:C₂₄H₂₆O₈
Molecular Weight:442.466
Hs Code.:

Synonyms:

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Chemical Property of 2,4-Di-O-Acetyl-1,3-O-benzyliden-α-D-tagatopyranose

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Technology Process of 2,4-Di-O-Acetyl-1,3-O-benzyliden-α-D-tagatopyranose

There total 7 articles about 2,4-Di-O-Acetyl-1,3-O-benzyliden-α-D-tagatopyranose which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 100-39-0
benzyl bromide

: 77387-31-6
2,4-Di-O-Acetyl-1,3-O-benzyliden-α-D-tagatopyranose

Guidance literature:: Multi-step reaction with 6 steps

1: BaO, Ba(OH)2*8H₂O / dimethylformamide / 48 h

2: LiAlH₄ / tetrahydrofuran / 24 h / Ambient temperature

3: 98 percent / RuO₂, K₂CO₃, NaIO₄ / CH₂Cl₂; H₂O / 7 h

4: LiAlH₄ / tetrahydrofuran / 0 degC to room temp.

5: 52 percent / 90percent CF₃COOH / 0.17 h / Ambient temperature

6: pyridine / 48 h / 60 °C

With ruthenium(IV) oxide; barium dihydroxide; sodium periodate; lithium aluminium tetrahydride; potassium carbonate; trifluoroacetic acid; barium(II) oxide; In tetrahydrofuran; pyridine; dichloromethane; water; N,N-dimethyl-formamide;

Reference yield:

: 72886-95-4
Methyl-5-O-benzyl-1,3-O-benzyliden-β-D-fructopyranosid

: 77387-31-6
2,4-Di-O-Acetyl-1,3-O-benzyliden-α-D-tagatopyranose

Guidance literature:: Multi-step reaction with 4 steps

1: 98 percent / RuO₂, K₂CO₃, NaIO₄ / CH₂Cl₂; H₂O / 7 h

2: LiAlH₄ / tetrahydrofuran / 0 degC to room temp.

3: 52 percent / 90percent CF₃COOH / 0.17 h / Ambient temperature

4: pyridine / 48 h / 60 °C

With ruthenium(IV) oxide; sodium periodate; lithium aluminium tetrahydride; potassium carbonate; trifluoroacetic acid; In tetrahydrofuran; pyridine; dichloromethane; water;

Reference yield:

: 77387-17-8,77387-21-4
Methyl-5-O-benzyl-1,3-O-benzyliden-β-D-threo-hexo-2,4-diulo-pyranosid

: 77387-31-6
2,4-Di-O-Acetyl-1,3-O-benzyliden-α-D-tagatopyranose

Guidance literature:: Multi-step reaction with 3 steps

1: LiAlH₄ / tetrahydrofuran / 0 degC to room temp.

2: 52 percent / 90percent CF₃COOH / 0.17 h / Ambient temperature

3: pyridine / 48 h / 60 °C

With lithium aluminium tetrahydride; trifluoroacetic acid; In tetrahydrofuran; pyridine;