1,3,5-tris{[(2'-furfurylaminoformyl)phenoxyl]methyl}-2,4,6-trimethylbenzene

Base Information

• Chemical Name: 1,3,5-tris{[(2'-furfurylaminoformyl)phenoxyl]methyl}-2,4,6-trimethylbenzene
• CAS No.: 1048637-33-7
• Molecular Formula: C₄₈H₄₅N₃O₉
• Molecular Weight: 807.9
• Mol file: 1048637-33-7.mol

Synonyms:

Chemical Property of 1,3,5-tris{[(2'-furfurylaminoformyl)phenoxyl]methyl}-2,4,6-trimethylbenzene

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 1,3,5-tris{[(2'-furfurylaminoformyl)phenoxyl]methyl}-2,4,6-trimethylbenzene

There total 1 articles about 1,3,5-tris{[(2'-furfurylaminoformyl)phenoxyl]methyl}-2,4,6-trimethylbenzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 87.0%

N-(furan-2-ylmethyl)-2-hydroxybenzamide (13156-92-8) + 1,3,5-tris(bromomethyl)-2,4,6-trimethylbenzene (21988-87-4) → 1,3,5-tris{[(2'-furfurylaminoformyl)phenoxyl]methyl}-2,4,6-trimethylbenzene (1048637-33-7)

Guidance literature:

With potassium carbonate; In acetone; for 12h; Heating;

DOI:10.1039/b800217g

Reference yield:

gadolinium(III) nitrate pentahydrate + 1,3,5-tris{[(2'-furfurylaminoformyl)phenoxyl]methyl}-2,4,6-trimethylbenzene (1048637-33-7) → [Gd(1,3,5-tris(((2'-furfurylaminoformyl)phenoxyl)methyl)-2,4,6-trimethylbenzene)(NO3)3]n

Guidance literature:

In methanol; ethyl acetate; layering ethyl acetate over soln. of furan deriv. in ethyl acetate, layering methanol soln. of gadolinium compd. over buffer layer, keeping for4-5 wks; collecting crystals, washing with ethyl acetate, drying in air, elem. anal.;

DOI:10.1039/b800217g

Reference yield:

praseodymium (III) nitrate * 5 water + 1,3,5-tris{[(2'-furfurylaminoformyl)phenoxyl]methyl}-2,4,6-trimethylbenzene (1048637-33-7) → (Pr(1,3,5-tris(((2'-furfurylaminoformyl)phenoxyl)methyl)-2,4,6-trimethylbenzene)(NO3)3*water)n

Guidance literature:

In methanol; ethyl acetate; layering ethyl acetate over soln. of furan deriv. in ethyl acetate, layering methanol soln. of praseodymium compd. over buffer layer, keeping for 4-5 wks; collecting crystals, washing with ethyl acetate, drying in air, elem. anal.;

DOI:10.1039/b800217g

upstream raw materials:

N-(furan-2-ylmethyl)-2-hydroxybenzamide

1,3,5-tris(bromomethyl)-2,4,6-trimethylbenzene