(2,6-dimesitylphenyl)(Ph)SbBr

Base Information

Chemical Name:(2,6-dimesitylphenyl)(Ph)SbBr
CAS No.:1052271-11-0
Molecular Formula:C₃₀H₃₀BrSb
Molecular Weight:592.222
Hs Code.:

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Chemical Property of (2,6-dimesitylphenyl)(Ph)SbBr

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Technology Process of (2,6-dimesitylphenyl)(Ph)SbBr

There total 1 articles about (2,6-dimesitylphenyl)(Ph)SbBr which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 35.0%

: 5035-52-9
dichlorophenylstibine

: (2,6-dimesitylphenyl)MgBr

: 1052271-11-0
(2,6-dimesitylphenyl)(Ph)SbBr

Guidance literature:: In tetrahydrofuran; (Ar); dropwise addn. of a soln. of Mg compd. to a soln. of Sb compd. in THF, stirring for 16 h at room temp.; evapn. in vac., extn. with toluene, cooling a soln. in benzene to -10°C; elem. anal.;
DOI:10.1016/j.jorganchem.2008.04.038

Reference yield: 60.0%

: 16853-85-3
lithium aluminium tetrahydride

: 1052271-11-0
(2,6-dimesitylphenyl)(Ph)SbBr

: 1052271-12-1
(2,6-dimesitylphenyl)(Ph)SbH

Guidance literature:: In diethyl ether; (Ar); dropwise addn. of a suspn. of Sb compd. in Et2O to a suspn. of LiAlH4 in Et2O at -50°C, stirring for 2 h; evapn. in vac., extn. with hexane, evapn.;
DOI:10.1016/j.jorganchem.2008.04.038

Reference yield: 19.3%

: 1052271-11-0
(2,6-dimesitylphenyl)(Ph)SbBr

: (2,6-dimesitylphenyl)(Ph)SbOH

Guidance literature:: With Al₂O₃; In toluene; (Ar); column chromy. of Sb compd. over Al2O3 with toluene; evapn.; elem. anal.;
DOI:10.1016/j.jorganchem.2008.04.038