N-[(2R,4aR,6R,7R,8R,8aS)-6-Allyloxy-2-phenyl-8-((2S,3S,4R,5R,6S)-3,4,5-tris-benzyloxy-6-methyl-tetrahydro-pyran-2-yloxy)-hexahydro-pyrano[3,2-d][1,3]dioxin-7-yl]-acetamide

Base Information

Chemical Name:N-[(2R,4aR,6R,7R,8R,8aS)-6-Allyloxy-2-phenyl-8-((2S,3S,4R,5R,6S)-3,4,5-tris-benzyloxy-6-methyl-tetrahydro-pyran-2-yloxy)-hexahydro-pyrano[3,2-d][1,3]dioxin-7-yl]-acetamide
CAS No.:211562-82-2
Molecular Formula:C₄₅H₅₁NO₁₀
Molecular Weight:765.901
Hs Code.:

N-[(2R,4aR,6R,7R,8R,8aS)-6-Allyloxy-2-phenyl-8-((2S,3S,4R,5R,6S)-3,4,5-tris-benzyloxy-6-methyl-tetrahydro-pyran-2-yloxy)-hexahydro-pyrano[3,2-d][1,3]dioxin-7-yl]-acetamide

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Chemical Property of N-[(2R,4aR,6R,7R,8R,8aS)-6-Allyloxy-2-phenyl-8-((2S,3S,4R,5R,6S)-3,4,5-tris-benzyloxy-6-methyl-tetrahydro-pyran-2-yloxy)-hexahydro-pyrano[3,2-d][1,3]dioxin-7-yl]-acetamide

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Technology Process of N-[(2R,4aR,6R,7R,8R,8aS)-6-Allyloxy-2-phenyl-8-((2S,3S,4R,5R,6S)-3,4,5-tris-benzyloxy-6-methyl-tetrahydro-pyran-2-yloxy)-hexahydro-pyrano[3,2-d][1,3]dioxin-7-yl]-acetamide

There total 6 articles about N-[(2R,4aR,6R,7R,8R,8aS)-6-Allyloxy-2-phenyl-8-((2S,3S,4R,5R,6S)-3,4,5-tris-benzyloxy-6-methyl-tetrahydro-pyran-2-yloxy)-hexahydro-pyrano[3,2-d][1,3]dioxin-7-yl]-acetamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 63064-48-2,116288-58-5,117299-90-8,126778-02-7,28738-44-5
allyl 2-acetamido-3,4,6-tri-O-acetyl-2-deoxy-β-D-glucopyranoside

: 211562-82-2
N-[(2R,4aR,6R,7R,8R,8aS)-6-Allyloxy-2-phenyl-8-((2S,3S,4R,5R,6S)-3,4,5-tris-benzyloxy-6-methyl-tetrahydro-pyran-2-yloxy)-hexahydro-pyrano[3,2-d][1,3]dioxin-7-yl]-acetamide

Guidance literature:: Multi-step reaction with 3 steps

1: NaOMe / methanol / 1 h / Ambient temperature

2: p-TsOH*H₂O / acetonitrile / 2 h / Ambient temperature

3: 4 Angstroem mol. sieves, Bu₄NBr / dimethylformamide; CH₂Cl₂ / 18 h

With 4 A molecular sieve; tetrabutylammomium bromide; sodium methylate; toluene-4-sulfonic acid; In methanol; dichloromethane; N,N-dimethyl-formamide; acetonitrile;
DOI:10.1016/S0008-6215(98)00066-4

Reference yield:

: 54400-75-8,64650-83-5,88903-97-3,116347-86-5,140849-88-3,144300-01-6,54400-77-0
allyl 2-acetamido-2-deoxy-β-D-glucopyranoside

: 211562-82-2
N-[(2R,4aR,6R,7R,8R,8aS)-6-Allyloxy-2-phenyl-8-((2S,3S,4R,5R,6S)-3,4,5-tris-benzyloxy-6-methyl-tetrahydro-pyran-2-yloxy)-hexahydro-pyrano[3,2-d][1,3]dioxin-7-yl]-acetamide

Guidance literature:: Multi-step reaction with 2 steps

1: p-TsOH*H₂O / acetonitrile / 2 h / Ambient temperature

2: 4 Angstroem mol. sieves, Bu₄NBr / dimethylformamide; CH₂Cl₂ / 18 h

With 4 A molecular sieve; tetrabutylammomium bromide; toluene-4-sulfonic acid; In dichloromethane; N,N-dimethyl-formamide; acetonitrile;
DOI:10.1016/S0008-6215(98)00066-4

Reference yield:

: 1125-88-8
benzaldehyde dimethyl acetal

: 211562-82-2
N-[(2R,4aR,6R,7R,8R,8aS)-6-Allyloxy-2-phenyl-8-((2S,3S,4R,5R,6S)-3,4,5-tris-benzyloxy-6-methyl-tetrahydro-pyran-2-yloxy)-hexahydro-pyrano[3,2-d][1,3]dioxin-7-yl]-acetamide

Guidance literature:: Multi-step reaction with 2 steps

1: p-TsOH*H₂O / acetonitrile / 2 h / Ambient temperature

2: 4 Angstroem mol. sieves, Bu₄NBr / dimethylformamide; CH₂Cl₂ / 18 h

With 4 A molecular sieve; tetrabutylammomium bromide; toluene-4-sulfonic acid; In dichloromethane; N,N-dimethyl-formamide; acetonitrile;
DOI:10.1016/S0008-6215(98)00066-4