PF₇₄-22

Base Information

Chemical Name:PF₇₄-22
CAS No.:1375277-91-0
Molecular Formula:C₂₆H₂₆N₄O₂
Molecular Weight:426.518
Hs Code.:

Synonyms:

Suppliers and Price of PF₇₄-22

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of PF₇₄-22

Chemical Property:

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Technology Process of PF₇₄-22

There total 5 articles about PF₇₄-22 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 4597-87-9
2-(N-methylamino)pyridine

: (2-(2-methyl-1H-indol-3-yl)acetyl)-D-phenylalanine

: 1375277-91-0
PF₇₄-22

Guidance literature:: With N-ethyl-N,N-diisopropylamine; N-[(dimethylamino)-3-oxo-1H-1,2,3-triazolo[4,5-b]pyridin-1-yl-methylene]-N-methylmethanaminium hexafluorophosphate; In N,N-dimethyl-formamide; at 70 ℃; for 16h;
DOI:10.1128/AAC.00646-15

Reference yield:

: 1912-43-2
2-methyl-3-indoleacetic acid

: 1375277-91-0
PF₇₄-22

Guidance literature:: Multi-step reaction with 3 steps

1: N-ethyl-N,N-diisopropylamine; N-[(dimethylamino)-3-oxo-1H-1,2,3-triazolo[4,5-b]pyridin-1-yl-methylene]-N-methylmethanaminium hexafluorophosphate / N,N-dimethyl-formamide / 2 h / 20 °C

2: sodium hydroxide / tetrahydrofuran / 12 h / 20 °C

3: N-ethyl-N,N-diisopropylamine; N-[(dimethylamino)-3-oxo-1H-1,2,3-triazolo[4,5-b]pyridin-1-yl-methylene]-N-methylmethanaminium hexafluorophosphate / N,N-dimethyl-formamide / 16 h / 70 °C

With N-ethyl-N,N-diisopropylamine; N-[(dimethylamino)-3-oxo-1H-1,2,3-triazolo[4,5-b]pyridin-1-yl-methylene]-N-methylmethanaminium hexafluorophosphate; sodium hydroxide; In tetrahydrofuran; N,N-dimethyl-formamide;
DOI:10.1128/AAC.00646-15

Reference yield:

: 2577-90-4
methyl (2S)-2-amino-3-phenylpropanoate

: 1375277-91-0
PF₇₄-22

Guidance literature:: Multi-step reaction with 3 steps

1: N-ethyl-N,N-diisopropylamine; N-[(dimethylamino)-3-oxo-1H-1,2,3-triazolo[4,5-b]pyridin-1-yl-methylene]-N-methylmethanaminium hexafluorophosphate / N,N-dimethyl-formamide / 2 h / 20 °C

2: sodium hydroxide / tetrahydrofuran / 12 h / 20 °C

3: N-ethyl-N,N-diisopropylamine; N-[(dimethylamino)-3-oxo-1H-1,2,3-triazolo[4,5-b]pyridin-1-yl-methylene]-N-methylmethanaminium hexafluorophosphate / N,N-dimethyl-formamide / 16 h / 70 °C

With N-ethyl-N,N-diisopropylamine; N-[(dimethylamino)-3-oxo-1H-1,2,3-triazolo[4,5-b]pyridin-1-yl-methylene]-N-methylmethanaminium hexafluorophosphate; sodium hydroxide; In tetrahydrofuran; N,N-dimethyl-formamide;
DOI:10.1128/AAC.00646-15