(C₅H₄N)2C₅H₂NC₆H₄CH₂OC₆H₃C₃HO₂CH₃

Base Information

• Chemical Name: (C₅H₄N)2C₅H₂NC₆H₄CH₂OC₆H₃C₃HO₂CH₃
• CAS No.: 1318265-76-7
• Molecular Formula: C₃₂H₂₃N₃O₃
• Molecular Weight: 497.553
• Mol file: 1318265-76-7.mol

Synonyms:

Chemical Property of (C₅H₄N)2C₅H₂NC₆H₄CH₂OC₆H₃C₃HO₂CH₃

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of (C₅H₄N)2C₅H₂NC₆H₄CH₂OC₆H₃C₃HO₂CH₃

There total 6 articles about (C₅H₄N)2C₅H₂NC₆H₄CH₂OC₆H₃C₃HO₂CH₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 44.0%

7-hydroxy-4-methyl-chromen-2-one (90-33-5,79566-13-5) + 4'-(4-bromomethylphenyl)-2,2':6',2''-terpyridine (89972-78-1) → (C5H4N)2C5H2NC6H4CH2OC6H3C3HO2CH3 (1318265-76-7)

Guidance literature:

With 18-crown-6 ether; potassium carbonate; In acetone; for 48h; Reflux; Inert atmosphere;

DOI:10.1002/ejic.201100125

Reference yield:

2-acetylpyridine (1122-62-9) → (C5H4N)2C5H2NC6H4CH2OC6H3C3HO2CH3 (1318265-76-7)

Guidance literature:

Multi-step reaction with 4 steps

1: iodine

2: methanol / Reflux

3: N-Bromosuccinimide; dibenzoyl peroxide / tetrachloromethane

4: 18-crown-6 ether; potassium carbonate / acetone / 48 h / Reflux; Inert atmosphere

With N-Bromosuccinimide; 18-crown-6 ether; iodine; potassium carbonate; dibenzoyl peroxide; In methanol; tetrachloromethane; acetone;

DOI:10.1002/ejic.201100125

Reference yield:

4-methyl-benzaldehyde (104-87-0) → (C5H4N)2C5H2NC6H4CH2OC6H3C3HO2CH3 (1318265-76-7)

Guidance literature:

Multi-step reaction with 4 steps

1: sodium hydroxide / ethanol

2: methanol / Reflux

3: N-Bromosuccinimide; dibenzoyl peroxide / tetrachloromethane

4: 18-crown-6 ether; potassium carbonate / acetone / 48 h / Reflux; Inert atmosphere

With N-Bromosuccinimide; 18-crown-6 ether; potassium carbonate; sodium hydroxide; dibenzoyl peroxide; In methanol; tetrachloromethane; ethanol; acetone;

DOI:10.1002/ejic.201100125

upstream raw materials:

2-acetylpyridine

7-hydroxy-4-methyl-chromen-2-one

4'-(4-bromomethylphenyl)-2,2':6',2''-terpyridine

1-(2-oxo-2-(2-pyridyl)ethyl)pyridinium iodide