Pyridine,2,2'-(1,3-propanediyl)bis-

Base Information

Chemical Name:Pyridine,2,2'-(1,3-propanediyl)bis-
CAS No.:15937-81-2
Molecular Formula:C13H14 N2
Molecular Weight:198.268
Hs Code.:
Mol file:15937-81-2.mol

Synonyms:Pyridine,2,2'-trimethylenedi- (6CI,8CI); 1,3-Bis(2-pyridyl)propane;1,3-Di(2-pyridyl)propane; NSC 278061

Suppliers and Price of Pyridine,2,2'-(1,3-propanediyl)bis-

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 16 raw suppliers

Chemical Property of Pyridine,2,2'-(1,3-propanediyl)bis-

Chemical Property:

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of Pyridine,2,2'-(1,3-propanediyl)bis-

There total 27 articles about Pyridine,2,2'-(1,3-propanediyl)bis- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 46.0%

: 100-69-6,25014-15-7,27476-03-5,329041-71-6
2-vinylpyridine

: 109-06-8
α-picoline

: 15937-81-2
1,3-bis(2-pyridyl)propane

Guidance literature:: α-picoline; With sodium; for 1h;

2-vinylpyridine; at 120 ℃; for 4h;
DOI:10.1021/jo034602n

Reference yield:

: 100-69-6,25014-15-7,27476-03-5,329041-71-6
2-vinylpyridine

: N-(α-methylbenzyl)-2-(pyridin-2-yl)ethylamine

: 15937-81-2
1,3-bis(2-pyridyl)propane

: 618-36-0
rac-methylbenzylamine

Guidance literature:: With n-butyllithium; In diethyl ether; hexane; at -89 - 20 ℃; for 16h;
DOI:10.1021/acs.organomet.8b00047

Reference yield:

: 100-69-6,25014-15-7,27476-03-5,329041-71-6
2-vinylpyridine

: 15937-81-2
1,3-bis(2-pyridyl)propane

Guidance literature:: Multi-step reaction with 2 steps

1: acetic acid / 16 h / Reflux

2: n-butyllithium / hexane; diethyl ether / 16 h / -89 - 20 °C

With n-butyllithium; acetic acid; In diethyl ether; hexane;
DOI:10.1021/acs.organomet.8b00047