Ag(C₅H₃N(CC₆H₅NC₆H₃(C(CH₃)3)2)2)⁽¹⁺⁾*OSO₂CF₃^(1-)*C₆H₅CH₃=Ag(C₅H₃N(CC₆H₅NC₆H₃(C(CH₃)3)2)2)(OSO₂CF₃)*C₆H₅CH₃

Base Information

• Chemical Name: Ag(C₅H₃N(CC₆H₅NC₆H₃(C(CH₃)3)2)2)⁽¹⁺⁾*OSO₂CF₃^(1-)*C₆H₅CH₃=Ag(C₅H₃N(CC₆H₅NC₆H₃(C(CH₃)3)2)2)(OSO₂CF₃)*C₆H₅CH₃
• CAS No.: 1307310-87-7
• Molecular Formula: CF₃O₃S*C₇H₈*C₄₇H₅₅AgN₃
• Molecular Weight: 1011.05

Synonyms:

Chemical Property of Ag(C₅H₃N(CC₆H₅NC₆H₃(C(CH₃)3)2)2)⁽¹⁺⁾*OSO₂CF₃^(1-)*C₆H₅CH₃=Ag(C₅H₃N(CC₆H₅NC₆H₃(C(CH₃)3)2)2)(OSO₂CF₃)*C₆H₅CH₃

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Technology Process of Ag(C₅H₃N(CC₆H₅NC₆H₃(C(CH₃)3)2)2)⁽¹⁺⁾*OSO₂CF₃^(1-)*C₆H₅CH₃=Ag(C₅H₃N(CC₆H₅NC₆H₃(C(CH₃)3)2)2)(OSO₂CF₃)*C₆H₅CH₃

There total 2 articles about Ag(C₅H₃N(CC₆H₅NC₆H₃(C(CH₃)3)2)2)⁽¹⁺⁾*OSO₂CF₃^(1-)*C₆H₅CH₃=Ag(C₅H₃N(CC₆H₅NC₆H₃(C(CH₃)3)2)2)(OSO₂CF₃)*C₆H₅CH₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 69.0%

2,6-bis[1-[(2,5-di-tert-butylphenyl)imino]-benzyl]pyridine (1218775-84-8) + silver trifluoromethanesulfonate (2923-28-6) + toluene (108-88-3,15644-74-3,16713-13-6) → Ag(C5H3N(CC6H5NC6H3(C(CH3)3)2)2)(1+)*OSO2CF3(1-)*C6H5CH3=Ag(C5H3N(CC6H5NC6H3(C(CH3)3)2)2)(OSO2CF3)*C6H5CH3 (1307310-87-7)

Guidance literature:

In toluene; (N2); addn. of silver salt to a soln. of ligand in toluene, stirring for14 h in the dark; cooling to -20°C, filtration, washing ppt. with hexanes, drying in vac., recrystn. by diffusion of hexanes into a satd. soln. in CDCl3 at-20°C; elem. anal.;

DOI:10.1039/c2dt12112c

Reference yield:

Ag(C5H3N(CC6H5NC6H3(C(CH3)3)2)2)(1+)*OSO2CF3(1-)*C6H5CH3=Ag(C5H3N(CC6H5NC6H3(C(CH3)3)2)2)(OSO2CF3)*C6H5CH3 (1307310-87-7) → Ag(C5H3N(CC6H5NC6H3(C(CH3)3)2)2)(CH3C6H5)(1+)*OSO2CF3(1-)=Ag(C5H3N(CC6H5NC6H3(C(CH3)3)2)2)(C6H5CH3)(OSO2CF3) (1307310-87-7)

Guidance literature:

In toluene; (N2); dissolving Ag complex in toluene, stirring for 1 h; filtration through Celite, diffusion of hexane at -30°C for several ds;

DOI:10.1039/c2dt12112c

Reference yield:

Ag(C5H3N(CC6H5NC6H3(C(CH3)3)2)2)(1+)*OSO2CF3(1-)*C6H5CH3=Ag(C5H3N(CC6H5NC6H3(C(CH3)3)2)2)(OSO2CF3)*C6H5CH3 (1307310-87-7) → Ag(C5H3N(CC6H5NC6H3(C(CH3)3)2)2)(CH3C6H5)(1+)*OSO2CF3(1-)=Ag(C5H3N(CC6H5NC6H3(C(CH3)3)2)2)(C6H5CH3)(OSO2CF3) (1307310-87-7)

Guidance literature:

In toluene; (N2); dissolving Ag complex in toluene, stirring for 1 h; filtration through Celite, diffusion of hexane at -30°C for several ds;

DOI:10.1039/c2dt12112c

upstream raw materials:

2,6-bis[1-[(2,5-di-tert-butylphenyl)imino]-benzyl]pyridine

silver trifluoromethanesulfonate

toluene

Downstream raw materials:

Ag(C₅H₃N(CC₆H₅NC₆H₃(C(CH₃)3)2)2)(C₅H₅N)⁽¹⁺⁾*OSO₂CF₃^(1-)=Ag(C₅H₃N(CC₆H₅NC₆H₃(C(CH₃)3)2)2)(C₅H₅N)(OSO₂CF₃)

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