3-O-(6-deoxy-6-sulfo-α-D-glucopyranosyl)-1,2-di-O-6-(4'-pentyl-[1,1'-biphenyl]-4-yl)hexanoylglycerol sodium

Base Information

Chemical Name:3-O-(6-deoxy-6-sulfo-α-D-glucopyranosyl)-1,2-di-O-6-(4'-pentyl-[1,1'-biphenyl]-4-yl)hexanoylglycerol sodium
CAS No.:1432064-40-8
Molecular Formula:C₅₅H₇₃O₁₂S*Na
Molecular Weight:981.233
Hs Code.:

Synonyms:

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Chemical Property of 3-O-(6-deoxy-6-sulfo-α-D-glucopyranosyl)-1,2-di-O-6-(4'-pentyl-[1,1'-biphenyl]-4-yl)hexanoylglycerol sodium

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Technology Process of 3-O-(6-deoxy-6-sulfo-α-D-glucopyranosyl)-1,2-di-O-6-(4'-pentyl-[1,1'-biphenyl]-4-yl)hexanoylglycerol sodium

There total 8 articles about 3-O-(6-deoxy-6-sulfo-α-D-glucopyranosyl)-1,2-di-O-6-(4'-pentyl-[1,1'-biphenyl]-4-yl)hexanoylglycerol sodium which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1432064-31-7
C₇₆H₉₁O₁₂S^(1-)*Na⁽¹⁺⁾

: 1432064-40-8
3-O-(6-deoxy-6-sulfo-α-D-glucopyranosyl)-1,2-di-O-6-(4'-pentyl-[1,1'-biphenyl]-4-yl)hexanoylglycerol sodium

Guidance literature:: With 20% palladium hydroxide-activated charcoal; hydrogen; In ethanol; at 20 ℃; for 16h;
DOI:10.1002/chem.201203296

Reference yield:

: 265312-93-4
1-O-allyl-2,3,4-tri-O-benzyl-6-deoxy-6-thioacetyl-α-D-glucopyranoside

: 1432064-40-8
3-O-(6-deoxy-6-sulfo-α-D-glucopyranosyl)-1,2-di-O-6-(4'-pentyl-[1,1'-biphenyl]-4-yl)hexanoylglycerol sodium

Guidance literature:: Multi-step reaction with 4 steps

1: AD-mix-α / tert-butyl alcohol; water / 22 h / 20 °C

2: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; dmap / dichloromethane / 20 h / 20 °C

3: acetic acid; Oxone; potassium acetate / 16 h / 20 °C

4: 20% palladium hydroxide-activated charcoal; hydrogen / ethanol / 16 h / 20 °C

With dmap; Oxone; AD-mix-α; 20% palladium hydroxide-activated charcoal; hydrogen; potassium acetate; acetic acid; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In ethanol; dichloromethane; water; tert-butyl alcohol;
DOI:10.1002/chem.201203296

Reference yield:

: 1432064-22-6
3-O-(2,3,4-tri-O-benzyl-6-deoxy-6-thioacetyl-α-D-glucopyranosyl)-1,2-di-O-6-(4'-pentyl-[1,1'-biphenyl]-4-yl)hexanoylglycerol

: 1432064-40-8
3-O-(6-deoxy-6-sulfo-α-D-glucopyranosyl)-1,2-di-O-6-(4'-pentyl-[1,1'-biphenyl]-4-yl)hexanoylglycerol sodium

Guidance literature:: Multi-step reaction with 2 steps

1: acetic acid; Oxone; potassium acetate / 16 h / 20 °C

2: 20% palladium hydroxide-activated charcoal; hydrogen / ethanol / 16 h / 20 °C

With Oxone; 20% palladium hydroxide-activated charcoal; hydrogen; potassium acetate; acetic acid; In ethanol;
DOI:10.1002/chem.201203296