(+)-13α-hydroxylupanine

Base Information

• Chemical Name: (+)-13α-hydroxylupanine
• CAS No.: 55820-85-4
• Molecular Formula: C₁₅H₂₄N₂O₂
• Molecular Weight: 264.368
• Mol file: 55820-85-4.mol

Synonyms:

Chemical Property of (+)-13α-hydroxylupanine

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of (+)-13α-hydroxylupanine

There total 12 articles about (+)-13α-hydroxylupanine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

1,5-diaminopentane dihydrochloride (1476-39-7) → (+)-angustifoline (550-43-6,82189-28-4,150283-69-5) + (+)-lupanine (6R,7S,9S,11S) (486-87-3,486-88-4,550-90-3,2665-89-6,4356-43-8,26438-61-9,72074-77-2) + (+)-13α-hydroxylupanine (6870-60-6,14694-14-5,15358-48-2,27773-60-0,55820-85-4,55869-89-1)

Guidance literature:

With Lupinus polyphyllus plant; In water; for 360h; feeding experiment with 13C labelled cadaverine;

Reference yield:

→ 13-Epihydroxy-α-isolupanin (6870-60-6,14694-14-5,15358-48-2,27773-60-0,55820-85-4,55869-89-1)

Guidance literature:

Keton (VIII), Hydrierung, PtO2, in A.;

Reference yield:

→ (+)-13α-hydroxylupanine (6870-60-6,14694-14-5,15358-48-2,27773-60-0,55820-85-4,55869-89-1)

Guidance literature:

Jamaicensin-hydrochlorid, wss. Formaldehyd, 3d, RT (Ausb. 51percent);

DOI:10.1021/jo01065a631

upstream raw materials:

1,5-diaminopentane dihydrochloride