Diphenylphosphino-dimethyl-aluminium

Base Information

Chemical Name:Diphenylphosphino-dimethyl-aluminium
CAS No.:85004-95-1
Molecular Formula:C₁₄H₁₆AlP
Molecular Weight:242.236
Hs Code.:

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Diphenylphosphino-dimethyl-aluminium

Chemical Property:

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Technology Process of Diphenylphosphino-dimethyl-aluminium

There total 2 articles about Diphenylphosphino-dimethyl-aluminium which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.0%

: 75-24-1
trimethylaluminum

: 829-85-6
diphenylphosphane

: 85004-95-1
Diphenylphosphino-dimethyl-aluminium

Guidance literature:: byproducts: CH4; heating (in tube sealed under Ar at -196°C) for 16 h at 160°C; extn. with toluene, ; washing with pentane;

Reference yield: 20.0%

: 865-37-2
dimethylaluminum hydride

: 829-85-6
diphenylphosphane

: 85004-95-1
Diphenylphosphino-dimethyl-aluminium

Guidance literature:: byproducts: H2; alane was distd. in vac. to PPh2H; 2 h at room temp, then heating at 90°C for 1 h; recrystn. from toluene;

Reference yield:

: 199620-14-9,13007-92-6
chromium⁽⁰⁾ hexacarbonyl

: 85004-95-1
Diphenylphosphino-dimethyl-aluminium

: Cr(CO)5(PPh₂AlMe₂)

Guidance literature:: In toluene; byproducts: CO; Me2AlPPh2, Cr(CO)6 and toluene heated at 110-140°C for 22 h; react. mixt. extd. with toluene, volatiles removed on vac. line, solvent vac. distilled;