C₁₃H₁₀ClF₂NO

Base Information

Chemical Name:C₁₃H₁₀ClF₂NO
CAS No.:1420683-88-0
Molecular Formula:C₁₃H₁₀ClF₂NO
Molecular Weight:269.678
Hs Code.:

C<sub>13</sub>H<sub>10</sub>ClF<sub>2</sub>NO

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₁₃H₁₀ClF₂NO

Chemical Property:

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Technology Process of C₁₃H₁₀ClF₂NO

There total 1 articles about C₁₃H₁₀ClF₂NO which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 89-98-5
2-chloro-benzaldehyde

: 3863-11-4
3,4-difluoroaniline

: 1420683-88-0
C₁₃H₁₀ClF₂NO

Guidance literature:: 3,4-difluoroaniline; With phenylborondichloride; In dichloromethane; at -30 - -20 ℃; for 0.5h;

2-chloro-benzaldehyde; In dichloromethane; at 20 ℃; for 4h;
DOI:10.1021/ml300351e

Reference yield:

: 1420683-88-0
C₁₃H₁₀ClF₂NO

: 1420683-99-3
2-allyl-9-(2-chlorophenyl)-7-fluoro-6-methoxy-1-methyl-2,4-dihydro-2,3,4,10-tetraazabenzo[f]azulene

Guidance literature:: Multi-step reaction with 3 steps

1: manganese(IV) oxide / dichloromethane / 4 h

2: sodium methylate / Inert atmosphere; Reflux

3: toluene-4-sulfonic acid / isopropyl alcohol / 15 h / 170 °C / Microwave irradiation

With manganese(IV) oxide; sodium methylate; toluene-4-sulfonic acid; In dichloromethane; isopropyl alcohol;
DOI:10.1021/ml300351e

Reference yield:

: 1420683-88-0
C₁₃H₁₀ClF₂NO

: 882531-87-5
R₁₅₃₀

Guidance literature:: Multi-step reaction with 4 steps

1: manganese(IV) oxide / dichloromethane / 4 h

2: sodium methylate / Inert atmosphere; Reflux

3: toluene-4-sulfonic acid / isopropyl alcohol / 15 h / 170 °C / Microwave irradiation

4: 1,3-bis[(diphenylphosphino)propane]dichloronickel(II); diisobutylaluminium hydride / tetrahydrofuran; toluene / 2 h / 0 °C

With manganese(IV) oxide; 1,3-bis[(diphenylphosphino)propane]dichloronickel(II); sodium methylate; diisobutylaluminium hydride; toluene-4-sulfonic acid; In tetrahydrofuran; dichloromethane; isopropyl alcohol; toluene;
DOI:10.1021/ml300351e