C₄₂H₄₅F₅O₂S₂

Base Information

Chemical Name:C₄₂H₄₅F₅O₂S₂
CAS No.:1443616-42-9
Molecular Formula:C₄₂H₄₅F₅O₂S₂
Molecular Weight:740.942
Hs Code.:

C<sub>42</sub>H<sub>45</sub>F<sub>5</sub>O<sub>2</sub>S<sub>2</sub>

Synonyms:

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Chemical Property of C₄₂H₄₅F₅O₂S₂

Chemical Property:

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Technology Process of C₄₂H₄₅F₅O₂S₂

There total 6 articles about C₄₂H₄₅F₅O₂S₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 111-83-1
1-bromo-octane

: 1443616-42-9
C₄₂H₄₅F₅O₂S₂

Guidance literature:: Multi-step reaction with 4 steps

1.1: potassium carbonate / acetonitrile / 1 h / 20 °C

1.2: 18 h / Reflux

2.1: trifluoroacetic acid; N-iodo-succinimide / acetonitrile / 48 h / Reflux

3.1: cesium fluoride; tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; triphenylphosphine / tetrahydrofuran / 72 h / 80 °C / Inert atmosphere

4.1: cesium fluoride; tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; triphenylphosphine / tetrahydrofuran / 24 h / 80 °C / Inert atmosphere

4.2: 2 h

With tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; N-iodo-succinimide; potassium carbonate; triphenylphosphine; cesium fluoride; trifluoroacetic acid; In tetrahydrofuran; acetonitrile; 4.1: |Stille Cross Coupling;
DOI:10.1002/chem.201203869

Reference yield:

: 344-04-7
bromopentafluorobenzene

: 1443616-42-9
C₄₂H₄₅F₅O₂S₂

Guidance literature:: Multi-step reaction with 4 steps

1.1: tetrakis(triphenylphosphine) palladium⁽⁰⁾ / tetrahydrofuran; N,N-dimethyl-formamide / 24 h / 80 °C / Inert atmosphere

2.1: n-butyllithium / tetrahydrofuran / 1 h / -78 °C / Inert atmosphere

2.2: 20 °C

3.1: cesium fluoride; tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; triphenylphosphine / tetrahydrofuran / 72 h / 80 °C / Inert atmosphere

4.1: cesium fluoride; tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; triphenylphosphine / tetrahydrofuran / 24 h / 80 °C / Inert atmosphere

4.2: 2 h

With tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; tetrakis(triphenylphosphine) palladium⁽⁰⁾; n-butyllithium; triphenylphosphine; cesium fluoride; In tetrahydrofuran; N,N-dimethyl-formamide; 1.1: |Stille Cross Coupling / 4.1: |Stille Cross Coupling;
DOI:10.1002/chem.201203869

Reference yield:

: 194204-71-2
2-bromo-1,4-bis(octyloxy)benzene

: 1443616-42-9
C₄₂H₄₅F₅O₂S₂

Guidance literature:: Multi-step reaction with 3 steps

1.1: trifluoroacetic acid; N-iodo-succinimide / acetonitrile / 48 h / Reflux

2.1: cesium fluoride; tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; triphenylphosphine / tetrahydrofuran / 72 h / 80 °C / Inert atmosphere

3.1: cesium fluoride; tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; triphenylphosphine / tetrahydrofuran / 24 h / 80 °C / Inert atmosphere

3.2: 2 h

With tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; N-iodo-succinimide; triphenylphosphine; cesium fluoride; trifluoroacetic acid; In tetrahydrofuran; acetonitrile; 3.1: |Stille Cross Coupling;
DOI:10.1002/chem.201203869