1-methyl-1-(6-phenyl-5-hexenyl)-hydrazine

Base Information

Chemical Name:1-methyl-1-(6-phenyl-5-hexenyl)-hydrazine
CAS No.:77172-41-9
Molecular Formula:C₁₃H₂₀N₂
Molecular Weight:204.315
Hs Code.:

Synonyms:

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Chemical Property of 1-methyl-1-(6-phenyl-5-hexenyl)-hydrazine

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Technology Process of 1-methyl-1-(6-phenyl-5-hexenyl)-hydrazine

There total 4 articles about 1-methyl-1-(6-phenyl-5-hexenyl)-hydrazine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 77153-80-1
1-amino-1-methyl-2-phenylperhydroazepinium iodide

: 77172-41-9
1-methyl-1-(6-phenyl-5-hexenyl)-hydrazine

: 49868-87-3
1-methyl-3-phenylperhydro-1,2-diazocine

Guidance literature:: With potassium tert-butylate; tert-butyl alcohol; In ethyl acetate; at 85 - 90 ℃; for 42h; Yield given. Yields of byproduct given. Title compound not separated from byproducts;
DOI:10.1021/jo00324a047

Reference yield:

: 3466-82-8
2-phenylazacycloheptane

: 77172-41-9
1-methyl-1-(6-phenyl-5-hexenyl)-hydrazine

Guidance literature:: Multi-step reaction with 4 steps

1: 88.5 percent / glacial acetic acid, hydrochlorid acid, NaNO₂ / H₂O / 1.) 0 deg C, 6 h, 2.) room temp., 12 h

2: 22.0 g / LiAlH₄ / diethyl ether / 16.5 h / Heating

3: 3.55 g / acetonitrile / 17 h / Heating

4: t-BuOK, t-BuOH / ethyl acetate / 42 h / 85 - 90 °C

With hydrogenchloride; lithium aluminium tetrahydride; potassium tert-butylate; acetic acid; tert-butyl alcohol; sodium nitrite; In diethyl ether; water; ethyl acetate; acetonitrile;
DOI:10.1021/jo00324a047

Reference yield:

: 77153-76-5
1-amino-2-phenylperhydroazepine

: 77172-41-9
1-methyl-1-(6-phenyl-5-hexenyl)-hydrazine

Guidance literature:: Multi-step reaction with 2 steps

1: 3.55 g / acetonitrile / 17 h / Heating

2: t-BuOK, t-BuOH / ethyl acetate / 42 h / 85 - 90 °C

With potassium tert-butylate; tert-butyl alcohol; In ethyl acetate; acetonitrile;
DOI:10.1021/jo00324a047