Technology Process of 1-methyl-1-(6-phenyl-5-hexenyl)-hydrazine
There total 4 articles about 1-methyl-1-(6-phenyl-5-hexenyl)-hydrazine which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
potassium tert-butylate; tert-butyl alcohol;
In
ethyl acetate;
at 85 - 90 ℃;
for 42h;
Yield given. Yields of byproduct given. Title compound not separated from byproducts;
DOI:10.1021/jo00324a047
- Guidance literature:
-
Multi-step reaction with 4 steps
1: 88.5 percent / glacial acetic acid, hydrochlorid acid, NaNO2 / H2O / 1.) 0 deg C, 6 h, 2.) room temp., 12 h
2: 22.0 g / LiAlH4 / diethyl ether / 16.5 h / Heating
3: 3.55 g / acetonitrile / 17 h / Heating
4: t-BuOK, t-BuOH / ethyl acetate / 42 h / 85 - 90 °C
With
hydrogenchloride; lithium aluminium tetrahydride; potassium tert-butylate; acetic acid; tert-butyl alcohol; sodium nitrite;
In
diethyl ether; water; ethyl acetate; acetonitrile;
DOI:10.1021/jo00324a047
- Guidance literature:
-
Multi-step reaction with 2 steps
1: 3.55 g / acetonitrile / 17 h / Heating
2: t-BuOK, t-BuOH / ethyl acetate / 42 h / 85 - 90 °C
With
potassium tert-butylate; tert-butyl alcohol;
In
ethyl acetate; acetonitrile;
DOI:10.1021/jo00324a047
