[IrRu(CO)4(bis(diphenylphosphino)methane)2][BF₄]

Base Information

• Chemical Name: [IrRu(CO)4(bis(diphenylphosphino)methane)2][BF₄]
• CAS No.: 323185-93-9
• Molecular Formula: BF₄*C₅₄H₄₄IrO₄P₄Ru
• Molecular Weight: 1260.93

Synonyms:

Chemical Property of [IrRu(CO)4(bis(diphenylphosphino)methane)2][BF₄]

Chemical Property:

Purity/Quality:

Safty Information:

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Technology Process of [IrRu(CO)4(bis(diphenylphosphino)methane)2][BF₄]

There total 1 articles about [IrRu(CO)4(bis(diphenylphosphino)methane)2][BF₄] which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

[IrRu(CO)3(μ-H)2(bis(diphenylphosphino)methane)2][BF4] + carbon monoxide (201230-82-2) → [IrRu(CO)4(bis(diphenylphosphino)methane)2][BF4] (323185-93-9)

Guidance literature:

In dichloromethane; byproducts: H2; complex suspn. stirred under CO for hours; pptd. (ether), recrystd. (CH2Cl2/ether), dried (vac.); elem. anal.;

Reference yield: 92.0%

diazomethane (186581-53-3,908094-01-9,334-88-3) + [IrRu(CO)4(bis(diphenylphosphino)methane)2][BF4] (323185-93-9) → [IrRu(CO)4(μ-CH2)(bis(diphenylphosphino)methane)2][BF4]

Guidance literature:

In dichloromethane; diazomethane bubbled through complex soln. for 30 min; concd. (Ar), pptd. (ether), recrystd. (CH2Cl2/ether), dried (vac.); elem. anal.;

Reference yield: 90.0%

[IrRu(CO)4(bis(diphenylphosphino)methane)2][BF4] (323185-93-9) + acetylene (74-86-2,25067-58-7) → [IrRu(CO)4(μ-C=CH2)(μ-Ph2PCH2PPh2)2][BF4]

Guidance literature:

In dichloromethane; (N2); std. Schlenk technique; soln. of Ir-Ru complex in CH2Cl2 was satd.with HCCH; stirred for 4 h under HCCH; Et2O added; pentane added; filtered; washed (Et2O); dried (vac.);

DOI:10.1021/om201201h

upstream raw materials:

carbon monoxide

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