3-(3'-methyl-2'-butenyl)phloroglucinaldehyde

Base Information

Chemical Name:3-(3'-methyl-2'-butenyl)phloroglucinaldehyde
CAS No.:77636-13-6
Molecular Formula:C₁₂H₁₄O₄
Molecular Weight:222.241
Hs Code.:

Synonyms:

Suppliers and Price of 3-(3'-methyl-2'-butenyl)phloroglucinaldehyde

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Total 2 raw suppliers

Chemical Property of 3-(3'-methyl-2'-butenyl)phloroglucinaldehyde

Chemical Property:

Purity/Quality:: 98% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

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Technology Process of 3-(3'-methyl-2'-butenyl)phloroglucinaldehyde

There total 1 articles about 3-(3'-methyl-2'-butenyl)phloroglucinaldehyde which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 115-18-4
2-methyl-3-buten-2-ol

: 487-70-7
2,4,6-trihydroxybenzaldehyde

: 77636-13-6
3-(3'-methyl-2'-butenyl)phloroglucinaldehyde

Guidance literature:: With boron trifluoride diethyl etherate; In 1,4-dioxane; for 1h; Ambient temperature;

Reference yield:

: 77636-13-6
3-(3'-methyl-2'-butenyl)phloroglucinaldehyde

: 4335-12-0
toddaculin

Guidance literature:: Multi-step reaction with 5 steps

1: 2.2 g / sodium acetate

2: 420 mg / aqueous ammonia / methanol / cold

3: 275 mg / K₂CO₃ / acetone

4: 200 mg / aqueous ammonia / methanol / 3 h / 60 °C

5: 120 mg / K₂CO₃ / acetone

With ammonium hydroxide; sodium acetate; potassium carbonate; In methanol; acetone;

Reference yield:

: 77636-13-6
3-(3'-methyl-2'-butenyl)phloroglucinaldehyde

: 77636-08-9
toddanone

Guidance literature:: Multi-step reaction with 7 steps

1: 2.2 g / sodium acetate

2: 420 mg / aqueous ammonia / methanol / cold

3: 275 mg / K₂CO₃ / acetone

4: 200 mg / aqueous ammonia / methanol / 3 h / 60 °C

5: 120 mg / K₂CO₃ / acetone

6: 70 mg / m-chloroperbenzoic acid / diethyl ether

7: 12 mg / BF₃*Et₂O / dimethylsulfoxide / 15 h / 100 °C

With ammonium hydroxide; boron trifluoride diethyl etherate; sodium acetate; potassium carbonate; 3-chloro-benzenecarboperoxoic acid; In methanol; diethyl ether; dimethyl sulfoxide; acetone;