Technology Process of C19H24O5
There total 5 articles about C19H24O5 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
(E)-1-(2-hydroxy-6-methoxy-4-(methoxymethoxy)phenyl)-3-(4-methoxyphenyl)prop-2-en-1-one;
With
chloroformic acid ethyl ester; triethylamine;
With
sodium tetrahydroborate;
DOI:10.1021/ol4021095
- Guidance literature:
-
Multi-step reaction with 5 steps
1.1: N-ethyl-N,N-diisopropylamine / dichloromethane / 1 h / 0 °C / Inert atmosphere
2.1: potassium carbonate / acetone / 10 h / 80 °C
3.1: hydrogenchloride; water / methanol / 12 h / 30 °C
4.1: sodium hydride / N,N-dimethyl-formamide; mineral oil / 0.17 h / 0 °C
4.2: Claisen-Schmidt Condensation / 12.67 h / 2 - 20 °C
5.1: triethylamine; chloroformic acid ethyl ester
With
hydrogenchloride; water; chloroformic acid ethyl ester; sodium hydride; potassium carbonate; triethylamine; N-ethyl-N,N-diisopropylamine;
In
methanol; dichloromethane; N,N-dimethyl-formamide; acetone; mineral oil;
4.1: |Claisen-Schmidt Condensation;
DOI:10.1021/ol4021095
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: potassium carbonate / acetone / 10 h / 80 °C
2.1: hydrogenchloride; water / methanol / 12 h / 30 °C
3.1: sodium hydride / N,N-dimethyl-formamide; mineral oil / 0.17 h / 0 °C
3.2: Claisen-Schmidt Condensation / 12.67 h / 2 - 20 °C
4.1: triethylamine; chloroformic acid ethyl ester
With
hydrogenchloride; water; chloroformic acid ethyl ester; sodium hydride; potassium carbonate; triethylamine;
In
methanol; N,N-dimethyl-formamide; acetone; mineral oil;
3.1: |Claisen-Schmidt Condensation;
DOI:10.1021/ol4021095
