Technology Process of C15H24ClN3
There total 4 articles about C15H24ClN3 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
(triphenylphosphine)gold(I) chloride;
In
[D3]acetonitrile;
at 70 ℃;
for 24h;
Temperature;
Inert atmosphere;
DOI:10.1021/jacs.5b08756
- Guidance literature:
-
Multi-step reaction with 2 steps
1: acetonitrile[1,3-bis(2,6-diisopropylphenyl)imidazol-2-ylidene]gold(I) hexafluoroantimonate; sodium bromide / [D3]acetonitrile / 30 h / 70 °C / Inert atmosphere
2: (triphenylphosphine)gold(I) chloride / [D3]acetonitrile / 24 h / 70 °C / Inert atmosphere
With
(triphenylphosphine)gold(I) chloride; acetonitrile[1,3-bis(2,6-diisopropylphenyl)imidazol-2-ylidene]gold(I) hexafluoroantimonate; sodium bromide;
In
[D3]acetonitrile;
DOI:10.1021/jacs.5b08756
- Guidance literature:
-
Multi-step reaction with 2 steps
1: acetonitrile[1,3-bis(2,6-diisopropylphenyl)imidazol-2-ylidene]gold(I) hexafluoroantimonate; sodium bromide / [D3]acetonitrile / 30 h / 70 °C / Inert atmosphere
2: (triphenylphosphine)gold(I) chloride / [D3]acetonitrile / 24 h / 70 °C / Inert atmosphere
With
(triphenylphosphine)gold(I) chloride; acetonitrile[1,3-bis(2,6-diisopropylphenyl)imidazol-2-ylidene]gold(I) hexafluoroantimonate; sodium bromide;
In
[D3]acetonitrile;
DOI:10.1021/jacs.5b08756
