Technology Process of C40H38N4O8
There total 11 articles about C40H38N4O8 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
triethylamine;
In
dichloromethane;
at 20 ℃;
DOI:10.1021/jo300230z
- Guidance literature:
-
Multi-step reaction with 3 steps
1: tetrabutyl ammonium fluoride; acetic acid / tetrahydrofuran / 0.5 h / 20 °C
2: sodium tris(acetoxy)borohydride / acetic acid; acetonitrile / 2 h / 20 °C
3: triethylamine / dichloromethane / 20 °C
With
tetrabutyl ammonium fluoride; sodium tris(acetoxy)borohydride; acetic acid; triethylamine;
In
tetrahydrofuran; dichloromethane; acetic acid; acetonitrile;
DOI:10.1021/jo300230z
- Guidance literature:
-
Multi-step reaction with 10 steps
1: sodium hydroxide / N,N-dimethyl-formamide / 70 °C
2: pyridine / dichloromethane / 20 °C
3: trifluoroacetic acid / 0.17 h / 20 °C
4: N-iodo-succinimide / N,N-dimethyl-formamide / 1 h / 20 °C
5: water; methylamine / methanol / 20 °C
6: triphenylphosphine; diethylazodicarboxylate / tetrahydrofuran / 1 h / 0 - 20 °C
7: triphenyl-arsane; palladium diacetate; silver carbonate / chloroform / Reflux
8: tetrabutyl ammonium fluoride; acetic acid / tetrahydrofuran / 0.5 h / 20 °C
9: sodium tris(acetoxy)borohydride / acetic acid; acetonitrile / 2 h / 20 °C
10: triethylamine / dichloromethane / 20 °C
With
pyridine; N-iodo-succinimide; triphenyl-arsane; tetrabutyl ammonium fluoride; water; palladium diacetate; sodium tris(acetoxy)borohydride; acetic acid; triethylamine; triphenylphosphine; silver carbonate; methylamine; trifluoroacetic acid; sodium hydroxide; diethylazodicarboxylate;
In
tetrahydrofuran; methanol; dichloromethane; chloroform; acetic acid; N,N-dimethyl-formamide; acetonitrile;
6: Mitsunobu reaction / 7: Heck coupling;
DOI:10.1021/jo300230z