Technology Process of C20H24F4N2O
There total 6 articles about C20H24F4N2O which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
palladium diacetate; lithium carbonate; silver carbonate; p-benzoquinone;
In
tetrahydrofuran; N,N-dimethyl-formamide;
at 100 ℃;
for 12h;
Inert atmosphere;
DOI:10.1021/ja207607s
- Guidance literature:
-
Multi-step reaction with 4 steps
1: hydrogenchloride; water / 1,4-dioxane / 20 °C
2: oxalyl dichloride / dichloromethane / 0 - 20 °C / Inert atmosphere
3: toluene / 12 h / Reflux
4: palladium diacetate; lithium carbonate; silver carbonate; p-benzoquinone / tetrahydrofuran; N,N-dimethyl-formamide / 12 h / 100 °C / Inert atmosphere
With
hydrogenchloride; oxalyl dichloride; water; palladium diacetate; lithium carbonate; silver carbonate; p-benzoquinone;
In
tetrahydrofuran; 1,4-dioxane; dichloromethane; N,N-dimethyl-formamide; toluene;
DOI:10.1021/ja207607s
- Guidance literature:
-
Multi-step reaction with 3 steps
1: ammonia / water; ethyl acetate / 6 h / 20 °C
2: toluene / 12 h / Reflux
3: palladium diacetate; lithium carbonate; silver carbonate; p-benzoquinone / tetrahydrofuran; N,N-dimethyl-formamide / 12 h / 100 °C / Inert atmosphere
With
ammonia; palladium diacetate; lithium carbonate; silver carbonate; p-benzoquinone;
In
tetrahydrofuran; water; ethyl acetate; N,N-dimethyl-formamide; toluene;
DOI:10.1021/ja207607s
