Technology Process of C37H58O7Si2
There total 15 articles about C37H58O7Si2 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
hydrogenchloride;
In
chloroform; water;
at 20 ℃;
for 1h;
DOI:10.3762/bjoc.8.82
- Guidance literature:
-
With
sodium hydrogencarbonate; 3-chloro-benzenecarboperoxoic acid;
In
dichloromethane;
at 0 - 20 ℃;
for 2h;
Inert atmosphere;
DOI:10.3762/bjoc.8.82
- Guidance literature:
-
Multi-step reaction with 7 steps
1.1: potassium carbonate / acetone / 18 h / Reflux
2.1: lithium aluminium tetrahydride / tetrahydrofuran / 0.17 h / 20 °C / Inert atmosphere
3.1: silver trifluoroacetate / chloroform / 1 h / 20 °C
4.1: pyridine / dichloromethane / 18 h / 20 °C
5.1: tris(dibenzylideneacetone)dipalladium(0) chloroform complex; sodium t-butanolate / toluene / Inert atmosphere
5.2: 20 h / 50 °C / Inert atmosphere
6.1: diisobutylaluminium hydride / hexane; dichloromethane / 0.58 h / -78 - 20 °C / Inert atmosphere
7.1: sodium hydrogencarbonate; 3-chloro-benzenecarboperoxoic acid / dichloromethane / 2 h / 0 - 20 °C / Inert atmosphere
With
pyridine; tris(dibenzylideneacetone)dipalladium(0) chloroform complex; lithium aluminium tetrahydride; silver trifluoroacetate; diisobutylaluminium hydride; sodium hydrogencarbonate; potassium carbonate; 3-chloro-benzenecarboperoxoic acid; sodium t-butanolate;
In
tetrahydrofuran; hexane; dichloromethane; chloroform; acetone; toluene;
DOI:10.3762/bjoc.8.82
